Electrochemical behaviour of 2-[4′-sulphonamoylphenyl]hydrazono-1,3-indanediones

被引：0
|
作者：
Jain, R [1 ]
Bhadauria, A [1 ]
机构：
[1] Jiwaji Univ, Sch Studies Chem, Gwalior 474011, India
来源：
OXIDATION COMMUNICATIONS | 2005年 / 28卷 / 02期
关键词：
2-[4 '-sulphonamoylphenyl]hydrazono-1,3-indanediones; differential pulse polarography; cyclic voltammetry; hydmzones;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Electrochemical behaviour of 2-[4'-sulphonamoylphenyl]hydrazono-1,3-indanediones was studied in the Britton-Robinson buffers of pH 2.5 to 12.0 at dropping mercury electrode and glassy carbon electrode. At dropping mercury electrode a cathodic differential pulse poiarographic peak is obtained in the pH range 2.5 to 6.5. Cyclic voltammograms exhibited a well defined, irreversible cathodic and anodic peak at glassy carbon electrode. At pH 6.5 and above the reduction peak exhibited a tendency to split into two peaks indicating that the 4e(-)/4H(+) reduction of 2[4'-sulphonamoylphenyl]hydrazono-1,3-indanediones occurs in two one-electron and one two-electron steps. Products of controlled potential electrolysis were characterised by elemental and spectral analysis.
引用
收藏
页码：411 / 423
页数：13
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