Single crystal formation by solid state reaction between 8-hydroxyquinoline and 2,4,5-trichlorophenol

被引:5
|
作者
Singh, NB [1 ]
Srivastava, A
Fröhlich, R
机构
[1] Gorakhpur Univ, Dept Chem, Gorakhpur 273009, Uttar Pradesh, India
[2] Univ Munster, Dept Organ Chem, D-4400 Munster, Germany
关键词
Solid state reactions;
D O I
10.1039/b001412p
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
8-Hydroxyquinoline reacts with 2,4,5-trichlorophenol in solution as well as in the solid state forming a 1:1 addition compound. In the solid state, reaction proceeds by the diffusion of 8-hydroxyquinoline into the crystal lattice of 2,4,5-trichlorophenol and the reaction product separates in the form of single crystals. The crystal structure of the reaction product has been determined by X-ray diffraction techniques and belongs to a monoclinic system.
引用
收藏
页码:838 / 842
页数:5
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