Chemical, rheological properties and microstructure of road asphalt prepared from deoiled asphalt, slurry oil and polymers

被引:11
作者
Xin, Xue [1 ]
Jiang, Hongguang [1 ]
Liang, Ming [1 ]
Yao, Zhanyong [1 ]
Zhang, Jizhe [1 ]
Luo, Weixin [2 ]
Zhang, Xiaomeng [3 ]
机构
[1] Shandong Univ, Sch Qilu Transportat, Jinan 250002, Peoples R China
[2] Beijing Oriental Yuhong Waterproof Technol Co Ltd, State Key Lab Special Funct Waterproof Mat, Beijing 100123, Peoples R China
[3] Shandong Acad Transportat Sci, Jinan 250002, Peoples R China
基金
中国博士后科学基金; 中国国家自然科学基金;
关键词
Deoiled asphalt; FCC slurry oil; Chemical composition; Rheological properties; Microstructure; STORAGE STABILITY; PERFORMANCE; RUBBER; BINDER;
D O I
10.1016/j.conbuildmat.2020.119571
中图分类号
TU [建筑科学];
学科分类号
0813 ;
摘要
The demand for high quality asphalt binder is continuously increasing in road construction and paving industry, most of which derives from vacuum distillation of petroleum. Meanwhile, deoiled asphalt (DOA) and slurry oil are the by-products of solvent deasphalting and fluid catalytic cracking (FCC) respectively. This paper developed high-quality road asphalt binder from DOA modified with FCC slurry oil and polymers. Different styrene-butadienestyrene (SBS) and crumb rubber (CR) were selected as polymer modifiers. The optimized blending ratio of DOA/slurry was determined. Moreover, the effects of various modifiers on rheological properties, low-temperature cracking resistance, and microstructure of the resulting asphalt were evaluated. The results indicated that the incorporation of FCC slurry oil results in a more reasonable chemical composition and the improved cracking resistance of the blends. For different structure of SBS, radial SBS is more efficient to enhance the high temperature performance of DOA/ slurry blends. The DOA/slurry with 10% CR shows the approximate value in viscosity, complex modulus and vertical bar G*vertical bar/sin delta in comparison of sample with 5% linear SBS, demonstrating significant effectiveness of CR on improving the high temperature performance of DOA/slurry. Linear SBS is a better candidate improving low temperature performance of DOA/slurry. The FTIR analysis indicated that the double bonds of SBS take part in the chemical cross-linking reaction, whereas CR improves property of asphalt only by physical interactions. Regarding to morphology, linear SBS presents the homogeneous dispersion in the form of cycle particles, whereas radial SBS displays a rather irregular form of polymer phase. CR phase shows elongated features and forms a continuous phase when reaching 20% content, which significantly reinforces the mechanical property of the asphalt. (C) 2020 Elsevier Ltd. All rights reserved.
引用
收藏
页数:11
相关论文
共 37 条
[1]  
[Anonymous], 2013, D5 ASTM ASTM INT
[2]  
[Anonymous], 2007, 12593IP80 CEN
[3]  
[Anonymous], 2015, Standard Test Method for Viscosity Determination of Asphalt at Elevated Temperatures Using a Rotational Viscometer
[4]  
[Anonymous], 2002, D113 ASTM ASTM INT
[5]  
[Anonymous], 2014, D36 ASTM ASTM INT
[6]  
[Anonymous], 2002, D7003 ASTM ASTM INT
[7]   Investigation of low-temperature properties of recycling of aged SBS modified asphalt binder [J].
Bai, Min .
CONSTRUCTION AND BUILDING MATERIALS, 2017, 150 :766-773
[8]  
Celoglu M.E., 2018, INT J PAVEMENT ENG, P1
[9]   Road Asphalt Prepared by High Softening Point De-oiled Asphalt From Residuum Solvent Deasphalting [J].
Cheng, J. ;
Xiang, L. ;
Li, Z. .
PETROLEUM SCIENCE AND TECHNOLOGY, 2014, 32 (21) :2575-2583
[10]   The Characteristics of Asphalt Modified With FCC Slurry Oil [J].
Cheng, J. ;
Xiang, L. ;
Liu, K. .
PETROLEUM SCIENCE AND TECHNOLOGY, 2014, 32 (24) :3010-3019