Microstructure, texture evolution and mechanical properties of multi-directional forged Mg-13Gd-4Y-2Zn-0.5Zr alloy under decreasing temperature

被引:56
作者
Dong, Beibei [1 ]
Zhang, Zhimin [1 ]
Yu, Jianmin [1 ]
Che, Xin [1 ]
Meng, Mu [1 ]
Zhang, Jinlu [1 ]
机构
[1] North Univ China, Coll Mat Sci & Engn, 3 Xueyuan Rd, Taiyuan 030051, Peoples R China
关键词
Mg-13Gd-4Ye2Zn-0.5Zr alloy; Multi-directional forging (MDF); Microstructure; Texture evolution; Mechanical properties; ZN-ZR ALLOY; MAGNESIUM ALLOY; MG ALLOY; GRAIN-SIZE; DYNAMIC RECRYSTALLIZATION; TENSILE PROPERTIES; ORDERED STRUCTURE; STRAIN-RATE; RARE-EARTH; BEHAVIOR;
D O I
10.1016/j.jallcom.2020.153776
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this study, homogenized Mg-13Gd-4Ye2Zn-0.5Zr alloys were applied to multi-directional forging (MDF) process at decreasing temperatures from 480 degrees C to 420 degrees C by 4 passes. The microstructure, texture evolution and mechanical properties of the alloys during the MDF process were investigated. The result showed that the average grain size was refined remarkably to 4.0 mm and the microstructure distribution became homogeneous after 3 passes with cumulative strain of 9. After 4 passes with cumulative strain of 12, the average grain size increases to 5.4 mm. It is observed that large number of dynamic recrystallized (DRXed) grains and spherical precipitated phases of Mg-5(Gd,Y,Zn) occurred during the MDF processing. The area fraction of DRXed grains was increased to 97.3% that can be regarded as achieving complete dynamic recrystallization (DRX) after 3 passes. The grain refinement was mainly caused by DRX, and the DRX was induced via particle stimulation nucleation (PSN) mechanism. Moreover, part of lamellar longperiod stacking ordered (LPSO) phases were kinked and brought about numerous kink bands during multi-directional forging (MDF) process, which had an important impact on the grain refinement. As the MDF passes and cumulative strain increase, the basal texture transformed from strong basal texture to a random distribution gradually. The maximum ultimate tensile strength (UTS) and tensile yield strength (TYS) were 399 MPa and 308 MPa after 3 passes. The maximum failure elongation (FE) was 18.1% after 4 passes. (C) 2020 Elsevier B.V. All rights reserved.
引用
收藏
页数:13
相关论文
共 57 条
[1]   Long-period ordered structure in a high-strength nanocrystalline Mg-1 at% Zn-2 at% Y alloy studied by atomic-resolution Z-contrast STEM [J].
Abe, E ;
Kawamura, Y ;
Hayashi, K ;
Inoue, A .
ACTA MATERIALIA, 2002, 50 (15) :3845-3857
[2]   Modification of texture and microstructure of magnesium alloy extrusions by particle-stimulated recrystallization [J].
Al-Samman, T. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2013, 560 :561-566
[3]  
[Anonymous], J MAT SCI
[4]  
[Anonymous], MAT LETT
[5]  
[Anonymous], MRS S P
[6]   Evolution of sub-micron grain size and weak texture in magnesium alloy Mg-3Al-0.4Mn by a modified multi-axial forging process [J].
Biswas, Somjeet ;
Suwas, Satyam .
SCRIPTA MATERIALIA, 2012, 66 (02) :89-92
[7]   Enhanced mechanical property of AZ31B magnesium alloy processed by multi-directional forging method [J].
Chen Cai ;
Song LingHui ;
Du XingHao ;
Wu BaoLin .
MATERIALS CHARACTERIZATION, 2017, 131 :72-77
[8]   Influence of texture and grain size on work hardening and ductility in magnesium-based alloys processed by ECAP and rolling [J].
del Valle, J. A. ;
Carreno, F. ;
Ruano, O. A. .
ACTA MATERIALIA, 2006, 54 (16) :4247-4259
[9]   Influence of Zn Content on Microstructure and Tensile Properties of Mg-Zn-Y-Nd Alloy [J].
Du, Bei-Ning ;
Hu, Zi-Yang ;
Sheng, Li-Yuan ;
Xu, Dao-Kui ;
Zheng, Yu-Feng ;
Xi, Ting-Fei .
ACTA METALLURGICA SINICA-ENGLISH LETTERS, 2018, 31 (04) :351-361
[10]  
Du Y, 2018, RARE METAL MAT ENG, V47, P1422, DOI 10.1016/S1875-5372(18)30144-9