Calcium and zirconium as texture modifiers during rolling and annealing of magnesium-zinc alloys

被引:92
作者
Bohlen, Jan [1 ]
Wendt, Joachim [1 ]
Nienaber, Maria [1 ]
Kainer, Karl Ulrich [1 ]
Stutz, Lennart [1 ]
Letzig, Dietmar [1 ]
机构
[1] Helmholtz Zentrum Geesthacht, Magnesium Innovat Ctr, D-21502 Geesthacht, Germany
关键词
Magnesium alloys; Sheet rolling; Microstructure; Texture; Recrystallisation; X-ray diffraction; Electron backscatter diffraction (EBSD); MG-Y ALLOYS; DYNAMIC RECRYSTALLIZATION; GRAIN-SIZE; DEFORMATION; TEMPERATURE; BEHAVIOR; SOLUTE; SHEET; 1ST-PRINCIPLES; FORMABILITY;
D O I
10.1016/j.matchar.2015.02.002
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Rolling experiments were carried out on a ternary Mg-Zn-Ca alloy and its modification with zirconium. Short time annealing of as-rolled sheets is used to reveal the microstructure and texture development. The texture of the as-rolled sheets can be characterised by basal pole figures with split peak towards the rolling direction (RD) and a broad transverse angular spread of basal planes towards the transverse direction (TD). During annealing the RD split peaks as well as orientations in the sheet plane vanish whereas the distribution of orientations tilted towards the TD remains. It is shown in EBSD measurements that during rolling bands of twin containing structures form. During subsequent annealing basal orientations close to the sheet plane vanish based on a grain nucleation and growth mechanism of recrystallisation. Orientations with tilt towards the TD remain in grains that do not undergo such a mechanism. The addition of Zr delays texture weakening. (C) 2015 Elsevier Inc. All rights reserved.
引用
收藏
页码:144 / 152
页数:9
相关论文
共 33 条
[1]   Application of texture simulation to understanding mechanical behavior of Mg and solid solution alloys containing Li or Y [J].
Agnew, SR ;
Yoo, MH ;
Tomé, CN .
ACTA MATERIALIA, 2001, 49 (20) :4277-4289
[2]   Sheet texture modification in magnesium-based alloys by selective rare earth alloying [J].
Al-Samman, T. ;
Li, X. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2011, 528 (10-11) :3809-3822
[3]   Texture Analysis with MTEX - Free and Open Source Software Toolbox [J].
Bachmann, F. ;
Hielscher, R. ;
Schaeben, H. .
TEXTURE AND ANISOTROPY OF POLYCRYSTALS III, 2010, 160 :63-+
[4]   TENSILE-COMPRESSIVE YIELD ASYMMETRIES IN HIGH-STRENGTH WROUGHT MAGNESIUM ALLOYS [J].
BALL, EA ;
PRANGNELL, PB .
SCRIPTA METALLURGICA ET MATERIALIA, 1994, 31 (02) :111-116
[5]   Influence of grain size on the compressive deformation of wrought Mg-3Al-1Zn [J].
Barnett, MR ;
Keshavarz, Z ;
Beer, AG ;
Atwell, D .
ACTA MATERIALIA, 2004, 52 (17) :5093-5103
[6]   On the influence of the grain size and solute content on the AE response of magnesium alloys tested in tension and compression [J].
Bohlen, Jan ;
Dobron, Patrik ;
Swiostek, Jacek ;
Letzig, Dietmar ;
Chmelik, Frantisek ;
Lukac, Pavel ;
Kainer, Karl Ulrich .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2007, 462 (1-2) :302-306
[7]   The texture and anisotropy of magnesium-zinc-rare earth alloy sheets [J].
Bohlen, Jan ;
Nuernberg, Marcus R. ;
Senn, Jeremy W. ;
Letzig, Dietmar ;
Agnew, Sean R. .
ACTA MATERIALIA, 2007, 55 (06) :2101-2112
[8]   Effect of rare earth elements on the microstructure and texture development in magnesium-manganese alloys during extrusion [J].
Bohlen, Jan ;
Yi, Sangbong ;
Letzig, Dietmar ;
Kainer, Karl Ulrich .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (26) :7092-7098
[9]   Acoustic emission study of the deformation behaviour of magnesium sheets [J].
Bohlen, Jan ;
Dobron, Patrik ;
Hantzsche, Kerstin ;
Letzig, Dietmar ;
Chmelik, Frantisek ;
Kainer, Karl Ulrich .
INTERNATIONAL JOURNAL OF MATERIALS RESEARCH, 2009, 100 (06) :790-795
[10]   Effects of Ca on Tensile Properties and Stretch Formability at Room Temperature in Mg-Zn and Mg-Al Alloys [J].
Chino, Yasumasa ;
Ueda, Takamichi ;
Otomatsu, Yuki ;
Sassa, Kensuke ;
Huang, Xinsheng ;
Suzuki, Kazutaka ;
Mabuchi, Mamoru .
MATERIALS TRANSACTIONS, 2011, 52 (07) :1477-1482