Analysis of volatile components of Lavandula luisieri L. by direct thermal desorption-gas chromatography-mass spectrometry

被引:56
作者
Sanz, J
Soria, AC
García-Vallejo, MC
机构
[1] CSIC, Inst Quim Organ Gen, E-28006 Madrid, Spain
[2] Inst Nacl Invest & Tecnol Agraria & Alimentaria, Ctr Invest Forestal, Madrid 28040, Spain
关键词
Lavandula luisieri; thermal desorption; volatile organic compounds; necrodanes;
D O I
10.1016/j.chroma.2003.10.024
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Volatile components of wild samples of Lavandula luisieri collected in Central and Southern Spain have been analyzed by direct thermal desorption coupled to gas chromatography-mass spectrometry (DTD-GC-MS). This method requires only 10-20 mg of dry sample, allowing to obtain qualitative and quantitative results from different plant parts such as flowers and leaves. Average volatile yield calculated from 51 individual plants was higher for leaves (9.7 mg g(-1)) than for flowers (2.9 mg g(-1)). Samples presented a high variation in their yield and composition. Major components were camphor and 1,8-cineole (up to 80.9 and 76.7% in leaves; 87.8 and 85.2% in flowers, respectively); however, these compounds were not detected in several samples. Other major component (up to 60% in flowers and leaves) was 2,3,5,5-tetramethyl-4-methylene-2-cyclopenten-1-one. Multivariate analysis was applied to quantitative data from nine selected compounds in order to show the presence of several patterns in plant composition which were only partially related to the site of collection. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:139 / 146
页数:8
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