AstroEBSD: exploring new space in pattern indexing with methods launched from an astronomical approach

被引:32
作者
Britton, Thomas Benjamin [1 ]
Tong, Vivian S. [1 ]
Hickey, Jim [1 ]
Foden, Alex [1 ]
Wilkinson, Angus J. [2 ]
机构
[1] Imperial Coll London, Dept Mat, London SW7 2AZ, England
[2] Univ Oxford, Dept Mat, Oxford OX1 3UJ, England
来源
JOURNAL OF APPLIED CRYSTALLOGRAPHY | 2018年 / 51卷
基金
英国工程与自然科学研究理事会;
关键词
electron Kikuchi diffraction; indexing; astronomy; scanning electron microscopy; electron backscatter diffraction; EBSD; ELECTRON BACKSCATTER DIFFRACTION; RELATE; 2; SETS; CRYSTAL ORIENTATIONS; DICTIONARY APPROACH; MATCHING ALGORITHM; LOCAL TEXTURE; EBSD; RESOLUTION; IDENTIFICATION; CALIBRATION;
D O I
10.1107/S1600576718010373
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Electron backscatter diffraction (EBSD) is a technique used to measure crystallographic features in the scanning electron microscope. The technique is highly automated and readily accessible in many laboratories. EBSD pattern indexing is conventionally performed with raw electron backscatter patterns. These patterns are software processed to locate the band centres (and sometimes edges) from which the crystallographic index of each band is determined. Once a consistent index for many bands is obtained, the crystal orientation with respect to a reference sample and detector orientation can be determined and presented. Unfortunately, because of challenges related to crystal symmetry, there are limited available pattern-indexing approaches and this has probably hampered open development of the technique. In this article, a new method of pattern indexing is presented, based upon a method with which satellites locate themselves in the night sky, and its effectiveness is systematically demonstrated using dynamical simulations and real experimental patterns. The benefit of releasing this new algorithm as open-source software is demonstrated when this indexing process is utilized, together with dynamical solutions, to provide some of the first accuracy assessments of an indexing solution. In disclosing a new indexing algorithm, and software processing toolkit, the authors hope to open up EBSD developments to more users. The software code and example data are released alongside this article for third party developments.
引用
收藏
页码:1525 / 1534
页数:10
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