Local and transient nanoscale strain mapping during in situ deformation

被引:45
作者
Gammer, C. [1 ,5 ]
Kacher, J. [1 ,2 ,6 ]
Czarnik, C. [3 ]
Warren, O. L. [4 ]
Ciston, J. [1 ]
Minor, A. M. [1 ,2 ]
机构
[1] Lawrence Berkeley Natl Lab, Natl Ctr Elect Microscopy Mol Foundry, Berkeley, CA 94720 USA
[2] Univ Calif Berkeley, Dept Mat Sci & Engn, Berkeley, CA 94720 USA
[3] Gatan Inc, Pleasanton, CA 94588 USA
[4] Hysitron Inc, Minneapolis, MN 55344 USA
[5] Erich Schmid Inst Mat Sci, Jahnstr 12, Leoben, Austria
[6] Georgia Inst Technol, Sch Mat Sci & Engn, Atlanta, GA 30332 USA
基金
奥地利科学基金会; 美国国家科学基金会;
关键词
ELECTRON-MICROSCOPY; TEM;
D O I
10.1063/1.4961683
中图分类号
O59 [应用物理学];
学科分类号
摘要
The mobility of defects such as dislocations controls the mechanical properties of metals. This mobility is determined both by the characteristics of the defect and the material, as well as the local stress and strain applied to the defect. Therefore, the knowledge of the stress and strain during deformation at the scale of defects is important for understanding fundamental deformation mechanisms. Here, we demonstrate a method of measuring local stresses and strains during continuous in situ deformation with a resolution of a few nanometers using nanodiffraction strain mapping. Our results demonstrate how large multidimensional data sets captured with high speed electron detectors can be analyzed in multiple ways after an in situ TEM experiment, opening the door for true multimodal analysis from a single electron scattering experiment. Published by AIP Publishing.
引用
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页数:5
相关论文
共 16 条
[1]   In situ synchrotron tomographic quantification of granular and intragranular deformation during semi-solid compression of an equiaxed dendritic Al-Cu alloy [J].
Cai, B. ;
Karagadde, S. ;
Yuan, L. ;
Marrow, T. J. ;
Connolley, T. ;
Lee, P. D. .
ACTA MATERIALIA, 2014, 76 :371-380
[2]   Diffraction contrast imaging using virtual apertures [J].
Gammer, Christoph ;
Ozdol, V. Burak ;
Liebscher, Christian H. ;
Minor, Andrew M. .
ULTRAMICROSCOPY, 2015, 155 :1-10
[3]   Mechanics and Dynamics of the Strain-Induced M1-M2 Structural Phase Transition in Individual VO2 Nanowires [J].
Guo, Hua ;
Chen, Kai ;
Oh, Y. ;
Wang, Kevin ;
Dejoie, Catherine ;
Asif, S. A. Syed ;
Warren, O. L. ;
Shan, Z. W. ;
Wu, J. ;
Minor, A. M. .
NANO LETTERS, 2011, 11 (08) :3207-3213
[4]  
Hertzberg RW., 1976, Deformation and Fracture Mechanics of Engineering Materials
[5]  
Hirth J.P., 1982, Theory of Dislocations
[6]   Measurement of the displacement field of dislocations to 0.03 Å by electron microscopy [J].
Hytch, MJ ;
Putaux, JL ;
Pénisson, JM .
NATURE, 2003, 423 (6937) :270-273
[7]   In situ synchrotron investigation of the deformation behavior of nanolamellar Ti5Si3/TiNi composite [J].
Jiang, Daqiang ;
Hao, Shijie ;
Zhang, Junsong ;
Liu, Yinong ;
Ren, Yang ;
Cui, Lishan .
SCRIPTA MATERIALIA, 2014, 78-79 :53-56
[8]   Combination of in situ straining and ACOM TEM: A novel method for analysis of plastic deformation of nanocrystalline metals [J].
Kobler, A. ;
Kashiwar, A. ;
Hahn, H. ;
Kuebel, C. .
ULTRAMICROSCOPY, 2013, 128 :68-81
[9]  
Minor AM, 2006, NAT MATER, V5, P697, DOI [10.1038/nmat1714, 10.1038/NMAT1714]
[10]   Scanning transmission electron microscopy strain measurement from millisecond frames of a direct electron charge coupled device [J].
Mueller, Knut ;
Ryll, Henning ;
Ordavo, Ivan ;
Ihle, Sebastian ;
Strueder, Lothar ;
Volz, Kerstin ;
Zweck, Josef ;
Soltau, Heike ;
Rosenauer, Andreas .
APPLIED PHYSICS LETTERS, 2012, 101 (21)