A new synthetic route of 4,4′-hexafluoroisopropylidene-2, 2-bis-(phthalic acid anhydride) and characterization of 4,4′-hexafluoroisopropylidene-2,2-bis-(phthalic acid anhydride)-containing polyimides

被引：8

作者：

Zhu, SZ ^{[1
]}

Zhao, JW ^{[1
]}

Zhang, YX ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Organ Chem, Shanghai 200032, Peoples R China

来源：

JOURNAL OF FLUORINE CHEMISTRY | 2003年 / 123卷 / 02期

关键词：

4,4 '-hexafluoroisopropylidene-2,2-bis-(phthalic acid anhydride); diamines; condensation; polyimides oligomers;

D O I：

10.1016/S0022-1139(03)00142-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The title product 4,4'-hexafluoroisopropylidene-2,2-bis-(phthalic acid anhydride) was prepared from hexafluoroacetone and o-xylene as the starting materials by condensation, oxidation and dehydration three-step reaction sequence. It reacted with diamines in DMF or xylene to give polyimides by condensation polymerization. Thermal and viscosity analyses show that these polyimides have lower molecular weight but excellent thermal stability. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：221 / 225

页数：5

共 50 条

[21] Inverse Gas Chromatographic Study of Sorption Thermodynamics in Thermally Rearranged Polymer Based on 2,2-Bis(3-amino-4-hydroxyphenyl)-hexafluoropropane and 4,4′-Hexafluoroisopropylidene Diphthalic Anhydride
Belov, Nikolay A.
Nizhegorodova, Yulia A.
Kim, Seungju
Han, Sang Hoon
Yampolskii, Yuri P.
Lee, Young Moo
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2013, 52 (31) : 10467 - 10475
[22] Amine-Templated Anionic Metal-Organic Frameworks with the 4,4′-(Hexafluoroisopropylidene) Bis(benzoic acid) Ligand
Wang, Xiqu
Liu, Lumei
Conato, Marlon
Jacobson, Allan J.
CRYSTAL GROWTH & DESIGN, 2011, 11 (06) : 2257 - 2263
[23] Comparative Kinetic Study and Microwaves Non-Thermal Effects on the Formation of Poly(amic acid) 4,4′-(Hexafluoroisopropylidene)diphthalic Anhydride (6FDA) and 4,4′-(Hexafluoroisopropylidene)bis(p-phenyleneoxy)dianiline (BAPHF). Reaction Activated by Microwave, Ultrasound and Conventional Heating
Mendoza Tellez, Hugo
Palacios Alquisira, Joaquin
Rius Alonso, Carlos
Lopez Cortes, Jose Guadalupe
Alvarez Toledano, Cecilio
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2011, 12 (10): : 6703 - 6721
[24] Packing effects in 4,4′-bis(4-hydroxybutyl)-2,2′-bipyridine and 4,4′-bis(4-bromobutyl)-2,2′-bipyridine
Iyer, VM
Stoeckli-Evans, H
D'Aléo, A
De Cola, L
Belser, P
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2005, 61 : O259 - O261
[25] New poly(amide imide imide)s based on tetraimide dicarboxylic acid condensed from 4,4′-(hexafluoroisopropylidene)diphthalic anhydride, m-aminobenzoic acid, and 4,4"-oxydianiline and various aromatic diamines
Yang, CP
Chen, RS
Hsu, MF
JOURNAL OF APPLIED POLYMER SCIENCE, 2003, 88 (03) : 669 - 679
[26] Synthesis and properties of organosoluble poly(amide imide imide)s based on tetraimide dicarboxylic acid condensed from 4,4′-(hexafluoroisopropylidene)diphthalic anhydride, 4,4′-oxydianiline, and trimellitic anhydride and various aromatic diamines
Yang, CP
Chen, RS
Wang, MJ
JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY, 2002, 40 (08) : 1092 - 1102
[27] Polymerization and characterization of 4,4′-bis(alkylsulfanyl)-2,2′-bithiophenes
Iarossi, D
Mucci, A
Schenetti, L
Seeber, R
Goldoni, F
MACROMOLECULES, 1999, 32 (05) : 1390 - 1397
[28] 4,4′-Bis(trimethylsilyl)-2,2′-bipyridine
Zheng, Chang-Ge
Cao, Hua-Peng
Song, Yang
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3144 - U407
[29] POLYIMIDES FROM 4,4'-(ALKYLENE-ALPHA,OMEGA-DIOXY) BIS(PHENYLSUCCINIC ANHYDRIDE)S AND BIS(PHENYLGLUTARIC ANHYDRIDE)S
TESHIROGI, T
JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY, 1989, 27 (02) : 653 - 660
[30] Microwave Assisted Polycondensation of Polyimides by [4,4′-(Hexafluoroisopropylidene)diphthalic anhydride, pyromellitic dianhydride] and [2,4,6-Trimethyl-m-phenylenediamine]. Power, Time, and Solvent Effect
Mendoza Tellez, Hugo
Palacios Alquisira, Joaquin
Guadalupe Lopez-Cortes, Jose
Alvarez-Toledano, Cecilio
JOURNAL OF APPLIED POLYMER SCIENCE, 2010, 116 (05) : 2816 - 2824

← 1 2 3 4 5 →