Synthesis of marigold-like ZnIn2S4 microspheres at low-temperature

被引:5
作者
Chand, Mool [1 ]
Rawat, A. S. [1 ]
Khanuja, Manika [2 ]
Rawat, Seema [3 ]
Ranwa, Mitesh [1 ]
机构
[1] HNB Garhwal Univ Srinagar, Dept Phys, Garhwal 246174, Uttarakhand, India
[2] Jamia Millia Islamia, Ctr Nanosci & Nanotechnol, New Delhi 110025, India
[3] Zakir Hussain Delhi Coll, Dept Phys, Jawahar Lal Nehru Marg, New Delhi 110002, India
关键词
ZnIn; 2; S; 4; Marigold-like microspheres; Low temperature; XPS;
D O I
10.1016/j.matpr.2021.09.345
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this paper, Zinc Indium Sulphide (ZnIn2S4) marigold like Microsphere are synthesized at 80 degrees C in aqueous solution by using Zinc sulphate ZnSO4, Indium sulphate In2(SO4)3 and Thioacetamide C2H5NS (TTA). We have characterized the nanopowder of the zinc Indium sulphide, by using various techniques, like UV-Vis spectrophotometer, Field emission scanning electron microscopy (FSEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). The variation of optical properties in Zinc Indium sulphide by using UV-visible spectroscopy, to find the energy band gap (2.31 eV). The hexagonal phase was confirmed from the X-ray diffraction pattern of ZnIn2S4. We have used a simple route to synthesize the Zinc Indium Sulphide, which involves, no templates, no organic solvents or surfactants, and at low temperature (80 degrees C). Our synthesized Zinc Indium Sulphide have got promising applications in a wide range of areas like solar energy conversion, electrical nanodevices, photocatalysis, optical devices, and electrical devices, etc. (c) 2021 Elsevier Ltd. All rights reserved. Selection and Peer-review under responsibility of the scientific committee of the Global Conference on Recent Advances in Sustainable Materials 2021.
引用
收藏
页码:2297 / 2300
页数:4
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