Ethyl 2-[1-(4-chlorophenyl)-2,5-dioxo-1,2,3,5-tetrahydroimidazo[1′,2′:1,2]-pyrimidino[5,4-b][1]benzofuran-3-yl]-acetate

被引:2
作者
Hu, Yang-Gen [1 ]
Zhu, Zheng-Rong [2 ]
Chen, Yu-Lu [3 ]
机构
[1] Yunyang Med Coll, Dept Med Chem, Shiyan 442000, Peoples R China
[2] Xiangfan Vocat & Tech Coll, Dept Med, Xiangfan 441021, Peoples R China
[3] Xianning Vocat & Tech Coll, Dept Chem, Xianning 437100, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词
D O I
10.1107/S1600536807066998
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The asymmetric unit of the title compound, C22H16ClN3O5, consists of two crystallographically independent molecules. The fused rings of the imidazo[1,2-a]benzo[4,5]furo[3,2-d] pyrimidine system are nearly coplanar and the chlorophenyl rings are twisted with respect to the two pyrimidinone ring systems by 71.00 (2) and 62.59 (2)degrees. The C atoms of the ethyl side chain are disordered and were refined using a split model. In the crystal structure, the molecules are connected via weak intra- and intermolecular C-H center dot center dot center dot O interactions are present. The ethyl group in one molecule is disordered over two positions, with site occupancy factors 0.55 and 0.45; in the other molecule only the methyl group is disordered over two positions, with site occupancy factors 0.6 and 0.4.
引用
收藏
页码:0321 / U5500
页数:16
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