Chemical synthesis, structural and magnetic properties of nano-structured Co-Zn-Fe-Cr ferrite

被引:86
作者
Alone, S. T. [1 ]
Shirsath, Sagar E. [1 ]
Kadam, R. H. [2 ]
Jadhav, K. M. [1 ]
机构
[1] Dr Babasaheb Ambedkar Marathwada Univ, Dept Phys, Aurangabad 431004, Maharashtra, India
[2] ShriKrishana Mahavidyalaya, Mat Res Lab, Gunjoti, Osmanabad MS, India
关键词
Nanostructured materials; Chemical synthesis; Magnetization; Transmission electron microscopy; TEM; Magnetic measurements; SOL-GEL; MAGNETOSTATIC INTERACTIONS; NANOPARTICLES; TEMPERATURE; BEHAVIOR;
D O I
10.1016/j.jallcom.2011.02.006
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Nanoparticles of Co1-xZnxFe2-xCrxO4 (x = 0.0-0.5) ferrites were prepared by chemical co-precipitation technique using metal sulphates. The structural and magnetic properties were investigated by means of X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), vibrating sample magnetometer (VSM), and AC susceptibility measurements. X-ray diffraction patterns indicate that the samples possess single phase cubic spinel structure. The lattice constant initially increases for x <= 0.3 and thereafter for x > 0.3 it decreases with increasing x. The saturation magnetization (Ms), magneton number (n(B)) and coercivity (Hc) decreases with increasing Cr-Zn content x. Curie temperature deduced from AC susceptibility data decreases with increasing x. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:5055 / 5060
页数:6
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