Synthesis and characterization of CoFe2O4 nanoparticles with high coercivity

被引:67
作者
Gandha, Kinjal [1 ]
Elkins, Kevin [1 ]
Poudyal, Narayan [1 ]
Liu, J. Ping [1 ]
机构
[1] Univ Texas Arlington, Dept Phys, Arlington, TX 76019 USA
关键词
COBALT-FERRITE NANOPARTICLES; MAGNETIC-PROPERTIES; RAMAN-SPECTROSCOPY; NANOCRYSTALS; NANOWIRES; STABILITY; FE;
D O I
10.1063/1.4916544
中图分类号
O59 [应用物理学];
学科分类号
摘要
Single crystalline CoFe2O4 nanoparticles with high coercivity were prepared via a one-step hydrothermal method. The shape and size of the nanocrystals (in the range of 20-100 nm) can be controlled by varying synthesis parameters such as the concentration of NaOH and CTAB. X-ray diffraction and Raman spectra analysis confirmed that all the as-synthesized nanoparticles have a face centered cubic spinel crystal structure. HRTEM observation of particles shows interlayer spacing 0.48 nm of (111) lattice planes. A coercive force up to 5.0 kOe and saturation magnetization of 73 emu/g was achieved at room temperature for the 40 nm CoFe2O4 nanoparticles. (C) 2015 AIP Publishing LLC.
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页数:4
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共 26 条
[1]   Cobalt and magnesium ferrite nanoparticles: Preparation using liquid foams as templates and their magnetic characteristics [J].
Bala, T ;
Sankar, CR ;
Baidakova, M ;
Osipov, V ;
Enoki, T ;
Joy, PA ;
Prasad, BLV ;
Sastry, M .
LANGMUIR, 2005, 21 (23) :10638-10643
[2]   Magnetic properties of cobalt ferrite-silica nanocomposites prepared by a sol-gel autocombustion technique [J].
Cannas, C. ;
Musinu, A. ;
Piccaluga, G. ;
Fiorani, D. ;
Peddis, D. ;
Rasmussen, H. K. ;
Morup, S. .
JOURNAL OF CHEMICAL PHYSICS, 2006, 125 (16)
[3]   Synthesis of high-coercivity cobalt ferrite nanocrystals [J].
Cedeno-Mattei, Y. ;
Perales-Perez, O. .
MICROELECTRONICS JOURNAL, 2009, 40 (4-5) :673-676
[4]   Novel method for synthesis of Fe core and C shell magnetic nanoparticles [J].
Chaudhary, Rakesh P. ;
Mohanty, Samarendra K. ;
Koymen, Ali R. .
CARBON, 2014, 79 :67-73
[5]   Unusually high coercivity and critical single-domain size of nearly monodispersed CoFe2O4 nanoparticles [J].
Chinnasamy, CN ;
Jeyadevan, B ;
Shinoda, K ;
Tohji, K ;
Djayaprawira, DJ ;
Takahashi, M ;
Joseyphus, RJ ;
Narayanasamy, A .
APPLIED PHYSICS LETTERS, 2003, 83 (14) :2862-2864
[6]   Stability of citrate-coated magnetite and cobalt-ferrite nanoparticles under laser irradiation: A Raman spectroscopy investigation [J].
da Silva, SW ;
Melo, TFO ;
Soler, MAG ;
Lima, ECD ;
da Silva, AF ;
Morais, PC .
IEEE TRANSACTIONS ON MAGNETICS, 2003, 39 (05) :2645-2647
[7]   High Energy Product Developed from Cobalt Nanowires [J].
Gandha, Kinjal ;
Elkins, Kevin ;
Poudyal, Narayan ;
Liu, Xubo ;
Liu, J. Ping .
SCIENTIFIC REPORTS, 2014, 4
[8]   Effect of RuCl3 on Morphology and Magnetic Properties of CoNi Nanowires [J].
Gandha, Kinjal ;
Poudyal, Narayan ;
Zhang, Qiang ;
Liu, J. Ping .
IEEE TRANSACTIONS ON MAGNETICS, 2013, 49 (07) :3273-3276
[9]   Synthesis of cobalt ferrite nanocrystallites by the forced hydrolysis method and investigation of their magnetic properties [J].
Hanh, N ;
Quy, OK ;
Thuy, NP ;
Tung, LD ;
Spinu, L .
PHYSICA B-CONDENSED MATTER, 2003, 327 (2-4) :382-384
[10]   Structural Investigation of MFe2O4 (M = Fe, Co) Magnetic Fluids [J].
Jacintho, Guilherme V. M. ;
Brolo, Alexandre G. ;
Corio, Paola ;
Suarez, Paulo A. Z. ;
Rubim, Joel C. .
JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 113 (18) :7684-7691