Influence of monomer type, plasticizer content, and powder/liquid ratio on setting characteristics of acrylic permanent soft denture liners based on poly(ethyl methacrylate/butyl methacrylate) and acetyl tributyl citrate

被引:4
|
作者
Mori, Tomoyasu [1 ]
Takase, Kazuma [1 ]
Yoshida, Kazuhiro [1 ]
Okazaki, Hitomi [1 ]
Murata, Hiroshi [1 ]
机构
[1] Nagasaki Univ, Grad Sch Biomed Sci, Dept Prosthet Dent, 1-7-1 Sakamoto, Nagasaki 8528588, Japan
关键词
Soft denture liners; Gelation time; Dynamic viscoelasticity; Acetyl tributyl citrate; Monomer; TISSUE CONDITIONERS; DYNAMIC VISCOELASTICITY; LINING MATERIALS; BOND STRENGTH; POLYMER; GELATION;
D O I
10.4012/dmj.2020-319
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
We evaluated the influence of monomer type, plasticizer content, and powder/liquid (P/L) ratio on the setting characteristics of light-cured acrylic permanent soft denture liners based on poly(ethyl methacrylate/butyl methacrylate). Two monomers, iso-butyl methacrylate (i-BMA) and 2-ethylhexyl methacrylate (2-EHMA), that contained various concentrations of the plasticizer acetyl tributyl citrate (ATBC) and trace amounts of the photo initiator and reducing agent were used. The P/L ratio was 1.0 or 1.2. The gelation time was measured using a controlled stress rheometer. Materials with i-BMA had shorter gelation times than those for materials with 2-EHMA. The gelation time increased exponentially with increasing plasticizer content. A higher P/L ratio led to a shorter gelation time. The effects of monomer type and plasticizer content were larger than that for the P/L ratio. These results show that 2-EHMA is a suitable monomer for soft denture liners and that the setting characteristics can be controlled via ATBC content.
引用
收藏
页码:918 / 927
页数:10
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