Preparation of WO3 nanorods with high specific surface area using double-walled carbon nanotubes as template

被引:4
作者
Yin, Yan-Hong [1 ,2 ]
Ma, Chun-An [1 ]
Wu, Zi-Ping [2 ]
Chen, Li-Tao [1 ]
Chu, You-Qun [1 ]
机构
[1] Zhejiang Univ Technol, Coll Chem Engn & Mat Sci, Int Sci & Technol Cooperat Base Energy Mat & Appl, State Key Lab Breeding Base Green Chem Synth Tech, Hangzhou 310032, Peoples R China
[2] Jiangxi Univ Sci & Technol, Sch Mat Sci & Engn, Minist Educ, Engn Res Ctr High Efficiency Dev & Applicat Techn, Ganzhou 341000, Peoples R China
基金
中国国家自然科学基金;
关键词
Tungsten oxide; Nanorods; Double-walled carbon nanotubes; Template; SINGLE-WALL; NANOPARTICLES; OXIDATION; GROWTH;
D O I
10.1007/s12598-015-0485-6
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The preparation of WO3 nanorods by double-walled carbon nanotube (DWCNT) template was investigated in this study. Owing to that the prepared H2WO4 can be isolated by the homogenously dispersed DWCNT bundles and secondary accumulation can be avoided effectively, the growth of H2WO4 can be restrained, and H2WO4 nanorods with diameter of 10-50 nm can be prepared. After calcination of the prepared DWCNT/H2WO4 composite in oxygen, WO3 nanorods with diameter of 10-100 nm and high specific surface area of 16.4 m(2).g(-1) can be obtained. It is concluded that the DWCNTs play an important role in the effective mediation of the morphology and size of nano-WO3.
引用
收藏
页码:1051 / 1056
页数:6
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