Preparative purification of coniferyl ferulate from Angelica sinensis oil by high performance centrifugal partition chromatography

被引：0
|
作者：
Yu, Yue [1 ]
Zhang, Qing-Wen [1 ]
Li, Shao-Ping [1 ]
机构：
[1] Univ Macau, Inst Chinese Med Sci, Taipa, Macau, Peoples R China
来源：
JOURNAL OF MEDICINAL PLANTS RESEARCH | 2011年 / 5卷 / 01期
关键词：
Angelica sinensis; coniferyl ferulate; high performance centrifugal partition chromatography; solvent extraction; COUNTER-CURRENT CHROMATOGRAPHY; LIQUID-CHROMATOGRAPHY; COMPONENTS; ACID; QUANTIFICATION; IDENTIFICATION; SEPARATION; EXTRACTION; ASSAY;
D O I：
暂无
中图分类号：
R914 [药物化学];
学科分类号：
100701 ;
摘要：
A high performance centrifugal partition chromatography (HPCPC) method was successfully developed to purify coniferyl ferulate (CF) from the extracts of commercial Angelica sinensis oil by using n-hexane-ethyl acetate-ethanol-water (5:5:5:5, v/v) as the two-phase solvent system. The upper and lower phases of this system were used as stationary and mobile phases, respectively. The purity of coniferyl ferulate was over 98% as determined by high-performance liquid chromatography (HPLC). The structure of coniferyl ferulate was identified by MS, H-1 NMR and C-13 NMR.
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收藏
页码：104 / 108
页数：5
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