[1] Univ Jaen, Linares High Polytech Sch EPSL, Dept Phys & Analyt Chem, Linares 23700, Spain
[2] Polytech Inst Braganca, Sch Agr, Mt Res Ctr CIMO, Braganca, Portugal
[3] Univ Porto, Fac Farm, REQUIMTE Lab Bromatol & Hidrol, P-4050313 Oporto, Portugal
[4] Almeria Univ, Dept Chem Engn, E-04071 Almeria, Spain