V2O5/SiO2 AS AN EFFICIENT CATALYST IN THE SYNTHESIS OF 5-AMINO-PYRAZOLE DERIVATIVES UNDER SOLVENT FREE CONDITION

被引：36

作者：

Khatab, Tamer K. ^{[1
]}

Hassan, Ashraf S. ^{[1
]}

Hafez, Taghrid S. ^{[1
]}

机构：

[1] Natl Res Ctr, Organometall & Organometalloid Chem Dept, Cairo 12622, Egypt

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2019年 / 33卷 / 01期

关键词：

One-pot synthesis; 5-Amino-1H-pyrazole; Hydrazine hydrate; Vanadium oxide; Silica; ROUTE;

D O I：

10.4314/bcse.v33i1.13

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An efficient and facile approach for the synthesis of 5-aminopyrazoles from ketene S,N-acetal and hydrazine hydrate via catalytic reaction under solvent free condition has been described. V2O5/SiO2 as a heterogeneous catalyst was prepared and characterized using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscope (SEM).

引用

页码：135 / 142

页数：8

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