Phenolic Profile Characterization of Chemlali Olive Stones by Liquid Chromatography-Ion Trap Mass Spectrometry

被引：33

作者：

Ben Mansour, Amir ^{[1
]}

Porter, Elaine A. ^{[2
]}

Kite, Geoffrey C. ^{[2
]}

Simmonds, Monique S. J. ^{[2
]}

Abdelhedi, Ridha ^{[1
]}

Bouaziz, Mohamed ^{[1
,3
]}

机构：

[1] Univ Sfax, Lab Electrochim & Environm, Ecole Natl Ingenieurs Sfax, Sfax 3038, Tunisia

[2] Royal Bot Gardens, Richmond TW9 3AB, Surrey, England

[3] Univ Sfax, Inst Super Biotechnol Sfax, Sfax 3038, Tunisia

来源：

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2015年 / 63卷 / 07期

关键词：

Chemlali olive stones; mass spectrometry; nuezhenide-11-methyl-oleoside; phenolic compounds; antioxidant activity; OLEA-EUROPAEA; DIODE-ARRAY; GLUCOSIDES; CULTIVAR; OILS; IDENTIFICATION; COMPOSITES; FLAVONOIDS; NUZHENIDE; QUALITY;

D O I：

10.1021/acs.jafc.5b00353

中图分类号：

S [农业科学];

学科分类号：

09 ;

摘要：

Aqueous methanol extracts of Chemlali olive stones were analyzed by reverse phase high-performance liquid chromatography (HPLC) with diode array detection and mass spectrometry [LC-MS/MS]. Oleoside, oleoside 11-methyl ester, nuezhenide, oleoside 11-methyloleoside, nuezhenide 11-methyloleoside, oleuropein, and glycosides of tryosol and hydroxytyrosol glycosides were identified in stones of Chemali olives. The antioxidant activity observed for the extract of the olive stones (IC50 = 13.84 mu g/mL, TEAC = 0.436 mM) may be due to the high content of phenolic compounds, of which the main compounds are nuezhenide (325.78 mg/100g), methoxy derivative of nuezhenide (132.46 mg/100g), and nuezhenide-11-methyloleoside (82.91 mg/100g). These results suggest the use of olive stones as sources of natural antioxidants.

引用

页码：1990 / 1995

页数：6

共 34 条

[1]

Abian J, 1999, J MASS SPECTROM, V34, P244, DOI 10.1002/(SICI)1096-9888(199904)34:4<244::AID-JMS775>3.0.CO

[2]

2-0

[3] Effect of Processing Systems on the Quality and Stability of Chemlali Olive Oils [J].

Ammar, Sonda ;

Zribi, Akram ;

Ben Mansour, Amir ;

Ayadi, Mohamed ;

Abdelhedi, Ridha ;

Bouaziz, Mohamed .

JOURNAL OF OLEO SCIENCE, 2014, 63 (04) :311-323

[4] Microcomponents of olive oil - III. Glucosides of 2(3,4-dihydroxy-phenyl)ethanol [J].

Bianco, A ;

Mazzei, RA ;

Melchioni, C ;

Romeo, G ;

Scarpati, ML ;

Soriero, A ;

Uccella, N .

FOOD CHEMISTRY, 1998, 63 (04) :461-464

[5] Identification and antioxidant potential of flavonoids and low molecular weight phenols in olive cultivar Chemlali growing in Tunisia [J].

Bouaziz, M ;

Grayer, RJ ;

Simmonds, MSJ ;

Damak, M ;

Sayadi, S .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2005, 53 (02) :236-241

[6] Removal of arsenic(III) from aqueous solution by activated carbons prepared from solvent extracted olive pulp and olive stones [J].

Budinova, T ;

Petrov, N ;

Razvigorova, M ;

Parra, J ;

Galiatsatou, P .

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2006, 45 (06) :1896-1901

[7]

Carraro L, 2005, ITAL J ANIM SCI, V4, P88

[8]

De Nino A, 1999, J MASS SPECTROM, V34, P10

[9] New Secoiridoid Glucosides from Ligustrum lucidum Induce ERK and CREB Phosphorylation in Cultured Cortical Neurons [J].

Fu, Guangmiao ;

Ip, Fanny C. F. ;

Pang, Haihong ;

Ip, Nancy Y. .

PLANTA MEDICA, 2010, 76 (10) :998-1003

[10] NEW SECOIRIDOID GLUCOSIDES FROM LIGUSTRUM-JAPONICUM [J].

FUKUYAMA, Y ;

KOSHINO, K ;

HASEGAWA, T ;

YAMADA, T ;

NAKAGAWA, K .

PLANTA MEDICA, 1987, (05) :427-431

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