Microwave-assisted palladium-catalysed carbonylations of aryl and heteroaryl halides with sulfamide nucleophiles utilising a solid CO source

被引：15

作者：

Liptrot, David ^{[1
]}

Alcaraz, Lilian ^{[1
]}

Roberts, Bryan ^{[1
]}

机构：

[1] AstraZeneca R&D Charnwood, Dept Chem, Loughborough LE11 5RH, Leics, England

来源：

TETRAHEDRON LETTERS | 2010年 / 51卷 / 40期

关键词：

Carbonylation; Palladium; Homogeneous catalysis; Microwave chemistry; Sulfamides; Acyl sulfamides; CARBON-MONOXIDE SOURCE; ENHANCED AMINOCARBONYLATIONS; PROMOTED AMINOCARBONYLATION; N-ARYL; MO(CO)(6); CHLORIDES; WATER;

D O I：

10.1016/j.tetlet.2010.08.009

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Mo(CO)(6) acts as a source of carbon monoxide for the palladium-catalysed, microwave-assisted, carbonylative coupling of aryl or heteroaryl halides with sulfamide nucleophiles to yield aryl and heteroaryl acyl sulfamides. Crown Copyright (C) 2010 Published by Elsevier Ltd. All rights reserved.

引用

页码：5341 / 5343

页数：3

共 23 条

[1] POTENTIAL ANTI-ATHEROSCLEROTIC AGENTS .3. SUBSTITUTED BENZOIC AND NON BENZOIC-ACID ANALOGS OF CETABEN [J].

ALBRIGHT, JD ;

DEVRIES, VG ;

DU, MT ;

LARGIS, EE ;

MINER, TG ;

REICH, MF ;

SHEPHERD, RG .

JOURNAL OF MEDICINAL CHEMISTRY, 1983, 26 (10) :1393-1411

[2] Novel N-aryl and N-heteroaryl sulfamide synthesis via palladium cross coupling [J].

Alcaraz, L ;

Bennion, C ;

Morris, J ;

Meghani, P ;

Thom, SM .

ORGANIC LETTERS, 2004, 6 (16) :2705-2708

[3]

GENTLES RG, 2007, Patent No. 2007275930

[4] Rapid palladium-catalyzed synthesis of esters from aryl halides utilizing Mo(CO)6 as a solid carbon monoxide source [J].

Georgsson, J ;

Hallberg, A ;

Larhed, M .

JOURNAL OF COMBINATORIAL CHEMISTRY, 2003, 5 (04) :350-352

[5] KINETICS AND MECHANISM OF SOLVOLYSIS OF N-ARYL SULFURIC DIAMIDES [J].

KAVALEK, J ;

KRALIKOVA, U ;

MACHACEK, V ;

SEDLAK, M ;

STERBA, V .

COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1990, 55 (01) :202-222

[6] Microwave-promoted aminocarbonylations of aryl chlorides using Mo(CO)6 as a solid carbon monoxide source [J].

Lagerlund, O ;

Larhed, M .

JOURNAL OF COMBINATORIAL CHEMISTRY, 2006, 8 (01) :4-6

[7] Microwave-promoted aminocarbonylation of aryl triflates using Mo(CO)6 as a solid CO source [J].

Odell, Luke R. ;

Savmarker, Jonas ;

Larhed, Mats .

TETRAHEDRON LETTERS, 2008, 49 (42) :6115-6118

[8]

Raboisson P. J. M. B., 2009, PCT Int. Appl., Patent No. [WO 2009080836A2 20090702, 2009080836]

[9]

RAVINDRANADH VS, 2006, J MED CHEM, V49, P31

[10] The role of sulfamide derivatives in medicinal chemistry: a patent review (2006-2008) [J].

Reitz, Allen B. ;

Smith, Garry R. ;

Parker, Michael H. .

EXPERT OPINION ON THERAPEUTIC PATENTS, 2009, 19 (10) :1449-1453

← 1 2 3 →