Analysis of Nb3Sn surface layers for superconducting radio frequency cavity applications

被引:36
作者
Becker, Chaoyue [1 ,2 ,3 ]
Posen, Sam [4 ]
Groll, Nickolas [1 ,2 ]
Cook, Russell [5 ]
Schlepuetz, Christian M. [6 ]
Hall, Daniel Leslie [4 ]
Liepe, Matthias [4 ,7 ]
Pellin, Michael [1 ]
Zasadzinski, John [3 ]
Proslier, Thomas [1 ,2 ]
机构
[1] Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USA
[2] Argonne Natl Lab, Div High Energy Phys, Argonne, IL 60439 USA
[3] IIT, Dept Phys, Chicago, IL 60616 USA
[4] Cornell Lab Accelerator Based Sci & Educ, Ithaca, NY 14853 USA
[5] Argonne Natl Lab, Nanosci & Technol Div, Argonne, IL 60439 USA
[6] Argonne Natl Lab, Xray Sci Div, Argonne, IL 60439 USA
[7] Cornell Univ, Dept Phys, Ithaca, NY 14853 USA
关键词
V3SI;
D O I
10.1063/1.4913617
中图分类号
O59 [应用物理学];
学科分类号
摘要
We present an analysis of Nb3Sn surface layers grown on a bulk Niobium (Nb) coupon prepared at the same time and by the same vapor diffusion process used to make Nb3Sn coatings on 1.3 GHz Nb cavities. Tunneling spectroscopy reveals a well-developed, homogeneous superconducting density of states at the surface with a gap value distribution centered around 2.7 +/- 0.4 meV and superconducting critical temperatures (T-c) up to 16.3 K. Scanning transmission electron microscopy performed on cross sections of the sample's surface region shows an similar to 2 mu m thick Nb3Sn surface layer. The elemental composition map exhibits a Nb:Sn ratio of 3:1 and reveals the presence of buried sub-stoichiometric regions that have a ratio of 5:1. Synchrotron x-ray diffraction experiments indicate a polycrystalline Nb3Sn film and confirm the presence of Nb rich regions that occupy about a third of the coating volume. These low Tc regions could play an important role in the dissipation mechanisms occurring during RF tests of Nb3Sn-coated Nb cavities and open the way for further improving a very promising alternative to pure Nb cavities for particle accelerators. (C) 2015 AIP Publishing LLC.
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页数:4
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