Box-Behnken experimental design for investigation of microwave-assisted extracted sugar beet pulp pectin

被引:61
作者
Li, De-qiang [1 ,2 ]
Jia, Xin [1 ,2 ]
Wei, Zhong [1 ,2 ]
Liu, Zhi-yong [1 ,2 ]
机构
[1] Shihezi Univ, Sch Chem & Chem Engn, Shihezi 832003, Xinjiang, Peoples R China
[2] Key Lab Green Proc Chem Engn Xinjiang Bintuan, Shihezi 832003, Xinjiang, Peoples R China
关键词
Microwave-assisted extraction; Sugar beet pulp pectin; Average molecular weight; Response surface methodology (RSM); Box-Behnken; RESPONSE-SURFACE METHODOLOGY; DRUG-DELIVERY; OPTIMIZATION; HYDROLYSIS; VISCOSITY;
D O I
10.1016/j.carbpol.2011.12.017
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Optimization of conditions for sugar beet pulp pectin (SBPP) extraction was investigated using response surface methodology (RSM). The average molecular weight ((M-t') over bar,) of twenty-nine SBPP samples was determined by viscometry. The relationships between four variables and two responses were studied using Box-Behnken experimental design. The constructed models were adequate to explain the relationships between independent variables and responses. All studied factors had great influence on the yield. The satisfactory conditions for SBPP extraction were obtained as follows: 152.63W of power, 3.53 min of time, 1.57 of pH of sulfuric and 18.92 of SLR. Among the studied factors, pH of sulfuric acid had the greatest influence on (M-t') over bar. (C) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码:342 / 346
页数:5
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