Synthesis and characterization of gold nanoparticles adsorbed in methyl cellulose micro fibrils

被引：13

作者：

Sahoo, Gobinda Prasad ^{[1
]}

Bhui, Dipak Kumar ^{[1
]}

Bar, Harekrishna ^{[1
]}

Sarkar, Priyanka ^{[1
]}

Samanta, Sadhan ^{[1
]}

Pyne, Santanu ^{[1
]}

Misra, Ajay ^{[1
]}

机构：

[1] Vidyasagar Univ, Dept Chem & Chem Technol, Midnapore 721102, WB, India

来源：

JOURNAL OF MOLECULAR LIQUIDS | 2010年 / 155卷 / 2-3期

关键词：

Gold nanoparticles; SPR; HRTEM; EDAX; XPS; SURFACE-PLASMON RESONANCE; SILVER NANOPARTICLES; CANCER; DIMENSIONS; MONOLAYERS; SCATTERING; CATALYSTS; CLUSTERS; SIZE; AU;

D O I：

10.1016/j.molliq.2010.05.013

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Methyl cellulose (MC) capped gold nanoparticles are successfully prepared through a simple route. Synthesis is based on the reduction of aqueous HAuCl4 center dot 4H(2)O by hydrogen gas at 85 degrees C and methyl cellulose has been used as encapsulating agent. Gold nanoparticle so-prepared are characterized by UV-Vis. X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and high resolution transmission electron microscopy (HRTEM). Methyl cellulose encapsulated gold hydrosol shows broad surface plasmon resonance (SPR) band with maxima at 537 nm along with a broad tail at 635 nm. In accordance with the SPR band, HRTEM micrograph shows two broad distributions of particles, most of them are small and spherical and nearly 25% particles are bigger with uneven shapes. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：91 / 95

页数：5

共 35 条

[1] Biosynthesis of gold nanoparticles by the tropical marine yeast Yarrowia lipolytica NCIM 3589
Agnihotri, Mithila
Joshi, Swanand
Kumar, Ameeta Ravi
Zinjarde, Smita
Kulkarni, Sulabha
[J]. MATERIALS LETTERS, 2009, 63 (15) : 1231 - 1234
[2] Gold-sulfur interactions in alkylthiol self-assembled monolayers formed on gold nanoparticles studied by solid-state NMR
Badia, A
Demers, L
Dickinson, L
Morin, FG
Lennox, RB
Reven, L
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (45) : 11104 - 11105
[3] Green synthesis of silver nanoparticles using seed extract of Jatropha curcas
Bar, Harekrishna
Bhui, Dipak Kr.
Sahoo, Gobinda P.
Sarkar, Priyanka
Pyne, Santanu
Misra, Ajay
[J]. COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2009, 348 (1-3) : 212 - 216
[4] Green synthesis of silver nanoparticles using latex of Jatropha curcas
Bar, Harekrishna
Bhui, Dipak Kr.
Sahoo, Gobinda R.
Sarkar, Priyanka
De, Sankar R.
Misra, Ajay
[J]. COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2009, 339 (1-3) : 134 - 139
[5] SMALL COLLOIDAL GOLD CONJUGATED TO FAB FRAGMENTS OR TO IMMUNOGLOBULIN-G AS HIGH-RESOLUTION LABELS FOR ELECTRON-MICROSCOPY - A TECHNICAL OVERVIEW
BASCHONG, W
WRIGLEY, NG
[J]. JOURNAL OF ELECTRON MICROSCOPY TECHNIQUE, 1990, 14 (04): : 313 - 323
[6] Synthesis and UV-vis spectroscopic study of silver nanoparticles in aqueous SDS solution
Bhui, Dipak Kumar
Bar, Harekrishna
Sarkar, Priyanka
Sahoo, Gobinda Prasad
De, Sankar Prasad
Misra, Ajay
[J]. JOURNAL OF MOLECULAR LIQUIDS, 2009, 145 (01) : 33 - 37
[7] Chemistry and properties of nanocrystals of different shapes
Burda, C
Chen, XB
Narayanan, R
El-Sayed, MA
[J]. CHEMICAL REVIEWS, 2005, 105 (04) : 1025 - 1102
[8] CHAN S, 2005, CHEM BIOL, V12, P323
[9] Recent advances in the liquid-phase syntheses of inorganic nanoparticles
Cushing, BL
Kolesnichenko, VL
O'Connor, CJ
[J]. CHEMICAL REVIEWS, 2004, 104 (09) : 3893 - 3946
[10] Surface plasmon resonance scattering and absorption of anti-EGFR antibody conjugated gold nanoparticles in cancer diagnostics: Applications in oral cancer
El-Sayed, IH
Huang, XH
El-Sayed, MA
[J]. NANO LETTERS, 2005, 5 (05) : 829 - 834

← 1 2 3 4 →