Preparation of Bi2S3 nanorods by microwave irradiation

被引：132
作者：
Liao, XH
Wang, H
Zhu, JJ [1 ]
Chen, HY
机构：
[1] Nanjing Univ, State Key Lab Coordinat Chem, Dept Chem, Nanjing 210093, Peoples R China
[2] Huazhong Normal Univ, Huangzhou 438000, Hubei, Peoples R China
来源：
MATERIALS RESEARCH BULLETIN | 2001年 / 36卷 / 13-14期
基金：
国家教育部科学基金资助; 中国国家自然科学基金;
关键词：
semiconductors; nanostructures; chemical synthesis; X-ray diffraction;
D O I：
10.1016/S0025-5408(01)00734-6
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Bi2S3 nanorods, with a diameter of ca. 10 nm and a length of up to ca. 300 nm, have been successfully prepared from a formaldehyde solution of bismuth nitrate and thiourea by microwave irradiation. Powder X-ray diffraction (XRD) pattern indicates that the product is pure orthorhombic Bi2S3 phase. The product is also characterized by the techniques of transmission electron microscopy (TEM) and X-ray photoelectron spectra (XPS). (C) 2001 Elsevier Science Ltd. All rights reserved.
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页码：2339 / 2346
页数：8
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