Discrimination of Semen cassiae from two related species based on the multivariate analysis of high-performance liquid chromatography fingerprints

被引:9
作者
Tang, Liying [1 ]
Wu, Hongwei [1 ]
Zhou, Xidan [1 ]
Xu, Yilong [1 ]
Zhou, Guohong [1 ]
Wang, Ting [1 ]
Kou, Zhenzhen [1 ]
Wang, Zhuju [1 ]
机构
[1] China Acad Chinese Med Sci, Inst Chinese Mat Med, Beijing 100700, Peoples R China
基金
中国国家自然科学基金;
关键词
Cassia obtusifolia L; Cassia tora L; High-performance liquid chromatography; Fingerprint analysis; Multivariate analysis; PURGATIVE CRUDE DRUGS; NAPHTHOPYRONE GLYCOSIDES; MASS-SPECTROMETRY; OBTUSIFOLIA L; SEEDS; ANTHRAQUINONES; TORA; CONSTITUENTS; SEPARATION; LINN;
D O I
10.1002/jssc.201500134
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A simple and efficient high-performance liquid chromatography fingerprint method was developed to discriminate Semen cassiae from two related species: Cassia obtusifolia L. (CO) and Cassia tora L. (CT), the seeds of which are abbreviated as COS and CTS, respectively. 22 major bioactive ingredients in 42 samples (20 COS and 22 CTS) collected from different provinces of China were identified. The statistical methods included similarity analysis and partial least-squares discriminant analysis. The pattern analysis method was specific and could be readily used for the comprehensive evaluation of Semen cassiae samples. Therefore, high-performance liquid chromatography fingerprint in combination with pattern analysis provided a simple and reliable method for discriminating between COS and CTS.
引用
收藏
页码:2431 / 2438
页数:8
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