[1] Univ Manchester, Sch Mat, Manchester M13 9PL, Lancs, England
[2] Kogi State Polytech, Dept Met, Itakpe, Nigeria
[3] Univ Witwatersrand, Sch Chem & Met Engn, ZA-2050 Johannesburg, South Africa
[4] Oxford Instruments NanoAnal, High Wycombe HP12 2SE, Bucks, England
[5] Univ Sao Paulo, Escola Politecn, Av Prof Mello Moraes 2463, Sao Paulo, SP, Brazil