Crystallographic alignment in the recombination stage in d-HDDR process of Nd-Fe-B-Ga-Nb powders

被引：12
作者：
Horikawa, Takashi [1 ]
Matsuura, Masashi [1 ]
Sugimoto, Satoshi [1 ]
Yamazaki, Masao [2 ]
Mishima, Chisato [2 ]
机构：
[1] Tohoku Univ, Grad Sch Engn, Dept Mat Sci, Sendai, Miyagi 9808579, Japan
[2] Aichi Steel Corp, Tokai, Aichi 4768666, Japan
来源：
AIP ADVANCES | 2016年 / 6卷 / 05期
关键词：
MICROSTRUCTURAL CHANGES; HYDROGEN ABSORPTION; DESORPTION; ALLOYS; DISPROPORTIONATION; ND16FE76B8; ANISOTROPY; INDUCEMENT; ND2FE14B; TEXTURE;
D O I：
10.1063/1.4944073
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Nd-Fe-B-Ga-Nb magnetic powder was subjected to the dynamic hydrogen disproportionation desorption recombination treatment. For samples disproportionated at both 30 and 100 kPa of hydrogen pressure, the changes in the microstructure and grain orientation during recombination process were investigated. It was observed that even during the recombination process, the orientation relationship was maintained between alpha-Fe and NdH2+x grains formed after the disproportionation treatment at 30 kPa of hydrogen pressure, [110]alpha-Fe // [110]NdH2+x, (-110)alpha-Fe // (-220) NdH2+x. Additionally, the alignment of recombined Nd2Fe14BHy grains became clear after 30 min of DR treatment showing following orientation relationship: (001) Nd2Fe14BHy // (110)alpha-Fe and (110)NdH2+x. In contrast, such a relationship was not observed in the sample disproportionated at 100 kPa of hydrogen pressure. This difference in the degree of alignment was also confirmed by measuring the magnetic property of the respective samples. (C) 2016 Author(s).
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页数：6
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