Microwave-assisted synthesis of nanosized MoSe2

被引：60
作者：
Harpeness, R
Gedanken, A [1 ]
Weiss, AM
Slifkin, MA
机构：
[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel
[2] Jerusalem Coll Technol, Dept Elect, IL-91160 Jerusalem, Israel
来源：
JOURNAL OF MATERIALS CHEMISTRY | 2003年 / 13卷 / 10期
关键词：
D O I：
10.1039/b303740a
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A microwave-assisted reaction between Mo(CO)(6) and Se has yielded MoSe2 nanoparticles. Nanorods of MoSe2 of lengths ranging from 45 to 55 nanometers are identified in the product mixture. The prepared MoSe2 has been characterized by X-ray powder diffraction measurements, FTIR spectroscopy, photoacoustic spectroscopy ( PAS), transmission electron microscopy (TEM) and high resolution TEM (HRTEM).
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页码：2603 / 2606
页数：4
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