One-Dimensional Barium Coordination Polymer With 2,2′-Bipyridine-5,5′-Dicarboxylate Ligand: Synthesis, Spectroscopic Characterization, Thermal Analyses, and Crystal Structure

被引:19
作者
Pour, Nasim Tadayon [1 ]
Khalighi, Aida [1 ]
Yousefi, Mohammad [1 ]
Amani, Vahid [1 ]
机构
[1] Islamic Azad Univ, Dept Chem, Yadegar E Imam Khomeini RAH Branch, Tehran, Iran
关键词
Ba(II); 2; 2'-bipyridine-5; 5'-dicarboxylic acid; crystal structure; thermal gravimetric; differential thermal analyses; luminescent properties; METAL-ORGANIC FRAMEWORKS; THIN-FILMS; COMPLEXES; ACID; 1,10-PHENANTHROLINE; DIVERSITY; IRON(III); CHLORIDE; HISTORY; IONS;
D O I
10.1080/15533174.2013.862822
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
[Ba(5,5 '-dcbipy)(-H2O)(2)(H2O)(2)](n) (1) complex was obtained from the reaction of one equivalent of 2,2'-bipyridine-5,5'-dicarboxylic acid (5,5 '-dcbipy.H-2) and one equivalent of ethylene diamine (en) with one equivalent of BaCl2.2H(2)O in water. This complex was characterized by elemental analysis, IR, UV-Vis, and luminescence spectroscopy and its structure was studied by the single-crystal X-ray diffraction method. The thermal stability of 1 was studied by thermogravimetric and differential thermal analyses.
引用
收藏
页码:1427 / 1433
页数:7
相关论文
共 42 条
[1]   Indium(III) hetero-ligand complexes containing 1,10-phenanthroline, chloride, acetonitrile and dimethyl sulfoxide: Crystal structure determination, and luminescent properties [J].
Abedi, Anita ;
Amani, Vahid ;
Safari, Nasser .
MAIN GROUP CHEMISTRY, 2012, 11 (03) :223-233
[2]   Indium(III) complexes containing bithiazole derivatives, chloride, methanol, and dimethyl sulfoxide: X-ray studies, spectroscopic characterization, and thermal analyses [J].
Abediy, Anita ;
Safari, Nasser ;
Amaniz, Vahid ;
Khavasiz, Hamid Reza .
JOURNAL OF COORDINATION CHEMISTRY, 2012, 65 (02) :325-338
[3]   Monomer and cyclic tetramer of copper(II) complexes: Synthesis, characterization and crystal structure determination of [Cu(dm4bt)Cl(Hipht)] and [{Cu(dm4bt)(H2O)(ipht)}4•2H2O] [J].
Al-Hashemi, Radhiya ;
Safari, Nasser ;
Amani, Saeid ;
Amani, Vahid ;
Khavasi, Hamid Reza .
POLYHEDRON, 2010, 29 (12) :2409-2416
[4]   Synthesis, characterization, and crystal structural study of the iron(II) 4,4'-bithiazole complex [Fe(C6H4N2S2)3]2+(NO3 -)2 [J].
Amani, Vahid ;
Abedi, Anita ;
Safari, Nasser .
MONATSHEFTE FUR CHEMIE, 2012, 143 (04) :589-593
[5]   Solution and solid state characterization of oxo-centered trinuclear iron(III) acetate complexes [Fe3(μ3-O)(μ-OAc)6(L)3]+ [J].
Amani, Vahid ;
Safari, Nasser ;
Khavasi, Hamid Reza .
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2012, 85 (01) :17-24
[6]   Synthesis, characterization and crystal structure determination of platinum(IV) complexes containing, bipyridine derivatives and chloride, [Pt(5,5′-dmbipy)Cl4] and [Pt(6-mbipy)Cl4] [J].
Amani, Vahid ;
Safari, Nasser ;
Khavasi, Hamid Reza ;
Akkurt, Mehmet .
POLYHEDRON, 2009, 28 (14) :3026-3030
[7]  
[Anonymous], MERC 1 4 1
[8]   Synchrotron study of poly[[di-μ-aqua(μ-2,2′-bipyridyl-5,5′-dicarboxylato)dipotassium] dihydrate] [J].
Bertke, Jeffrey A. ;
Oliver, Allen G. ;
Henderson, Kenneth W. .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 :M1265-+
[9]  
Blake AJ, 2010, NAT CHEM, V2, P688, DOI [10.1038/NCHEM.681, 10.1038/nchem.681]
[10]   Synthesis and Structural Diversity of Barium (N,N-Dimethylamino)diboranates [J].
Daly, Scott R. ;
Bellott, Brian J. ;
Nesbit, Mark A. ;
Girolami, Gregory S. .
INORGANIC CHEMISTRY, 2012, 51 (12) :6449-6459