Synthesis and structure of 1:1 complex of dimethyltin dichloride with meso-1,2-bis(alpha-diethoxyphosphorylbenzylamino)ethane

被引：13

作者：

Lorberth, J

Wocadlo, S

Massa, W

Grigoriev, EV

Yashina, NS

Petrosyan, VS

Finocchiaro, P

机构：

[1] MOSCOW MV LOMONOSOV STATE UNIV,DEPT CHEM,MOSCOW 119899,RUSSIA

[2] UNIV CATANIA,I-95125 CATANIA,ITALY

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 1996年 / 510卷 / 1-2期

关键词：

tin; phosphoryl ligand; crystal structure;

D O I：

10.1016/0022-328X(95)05894-U

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The crystal and molecular structure of the title compound has been determined by single crystal X-ray analysis. The complex is polymeric, the ligand coordinating in a bridging mode via two phosphoryl groups. The coordination environment at tin is octahedral with two methyl groups, two chlorine and two oxygen atoms occupying trans positions.

引用

收藏

页码：287 / 290

页数：4

相关论文

共 13 条

[1]

ASLANOV LA, 1977, ZH STRUKT KHIM, V18, P1103

[2]

CACCAMESE S, 1992, J CHEM RES-S, P242

[3] SN-119 NMR-STUDIES ON DIORGANOYLTIN(IV)DIHALIDES AND TRIORGANOYLTIN(IV)HALIDES - FORMATION AND STEREOCHEMISTRY OF ADDUCTS [J].

COLTON, R ;

DAKTERNIEKS, D .

INORGANICA CHIMICA ACTA, 1988, 148 (01) :31-36

[4]

CROMER DT, 1992, INT TABLES XRAY CRYS, VC

[5] STRUCTURAL INVESTIGATION ON 1-AMINO-ARYL-METHYLPHOSPHONATE ESTERS - X-RAY STRUCTURE OF O,O-DIETHYL-N-N'-ETHYLENE-BIS-PHENYLMETHYLPHOSPHONATE [J].

FAILLA, S ;

FINOCCHIARO, P ;

BELSKY, VK ;

ZAVODNIK, VE ;

SOBOLEV, AN .

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1993, 80 (1-4) :75-80

[6]

GRIGOREV EV, 1992, KOORDINATS KHIM+, V18, P1150

[7] ORGANOTIN(IV) COMPLEXES WITH TETRAETHYL ETHYLENE-DIPHOSPHONATE AND PROPYLENE-DIPHOSPHONATE [J].

GRIGORIEV, EV ;

YASHINA, NS ;

PRISCHENKO, AA ;

LIVANTSOV, MV ;

PETROSYAN, VS ;

MASSA, W ;

HARMS, K ;

WOCADLO, S ;

PELLERITO, L .

APPLIED ORGANOMETALLIC CHEMISTRY, 1995, 9 (01) :11-22

[8] INVESTIGATION INTO DIPHOSPHINE OXIDES AS LIGANDS IN DIORGANOTIN(IV) ADDUCTS .1. SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATION OF 1,2-BIS(DIPHENYLPHOSPHORYL)ETHANE TIN COMPLEXES AND X-RAY STRUCTURE OF [1,2-BIS(DIPHENYLPHOSPHORYL)ETHANE]DI-NORMAL-BUTYLDICHLOROTIN(IV) [J].

HARRISON, PG ;

SHARPE, NW ;

PELIZZI, C ;

PELIZZI, G ;

TARASCONI, P .

JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1983, (05) :921-926

[9] (ME2NCH[(ETO)2P=O]2.ME2SNCL2)-DIMER - CRYSTAL-STRUCTURE OF A BINUCLEAR BIS(CHELATE) COMPLEX OF TIN(IV) WITH CIS-LINKED OCTAHEDRA [J].

LORBERTH, J ;

SHIN, SH ;

OTTO, M ;

WOCADLO, S ;

MASSA, W ;

YASHINA, NS .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1991, 407 (03) :313-318

[10] SYNTHESIS AND STRUCTURE OF DIETHYLTINDICHLORIDE METHYLENEDIPHOSPHINATO COMPLEX - ET2SNCL2-CENTER-DOT[ME((I)PRO)P(O)]2CH2 [J].

LORBERTH, J ;

WOCADLO, S ;

MASSA, W ;

YASHINA, NS ;

GRIGOREV, EV ;

PETROSYAN, VS .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1994, 480 (1-2) :163-166