Synthesis, growth, crystal structure and characterization of a new organic material: Glycine glutaric acid

被引：32

作者：

Riscob, B. ^{[1
,2
]}

Shakir, Mohd. ^{[1
,2
]}

Sundar, J. Kalyana ^{[3
]}

Natarajan, S. ^{[3
]}

Wahab, M. A. ^{[2
]}

Bhagavannarayana, G. ^{[1
]}

机构：

[1] Natl Phys Lab CSIR, New Delhi 110012, India

[2] Jamia Millia Islamia, Crystal Growth Lab, Dept Phys, New Delhi 110025, India

[3] Madurai Kamaraj Univ, Sch Phys, Madurai 625021, Tamil Nadu, India

来源：

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2011年 / 78卷 / 01期

关键词：

Solubility; Growth from solution; Crystal structure; Organic compound; FT-IR spectroscopy; SINGLE-CRYSTALS; ENHANCEMENT; DIFFRACTION; PERFECTION; DEFECTS; ZTS;

D O I：

10.1016/j.saa.2010.11.026

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

Glycine glutaric acid, a new organic compound has been synthesized and good quality single crystals were grown by slow evaporation technique. The structure of the grown crystal was elucidated by using single crystal XRD. The presence of the functional groups was confirmed by using FT-IR spectroscopy. The optical transparency was studied by using UV-vis spectrophotometer and it was found that the crystal is having high optical transparency. The thermal stability of the crystal was studied by using thermo-gravimetric and differential thermal analyses and found that it is stable up to 150 degrees C. The room temperature dielectric studies were also carried out over the wide frequency range: 10 mHz to 10 MHz. (C) 2010 Elsevier B.V. All rights reserved.

引用

页码：543 / 548

页数：6

共 21 条

[1]

[Anonymous], 1990, Organic Superconductors

[2] Bis(glycine) lithium nitrate - A new non-centrosymmetric crystal: X-ray structure, vibrational spectra and DSC investigations [J].

Baran, J. ;

Drozd, M. ;

Ratajczak, H. ;

Pietraszko, A. .

JOURNAL OF MOLECULAR STRUCTURE, 2009, 927 (1-3) :43-53

[3] DYNAMICAL DIFFRACTION OF X RAYS BY PERFECT CRYSTALS [J].

BATTERMAN, BW ;

COLE, H .

REVIEWS OF MODERN PHYSICS, 1964, 36 (03) :681-&

[4] Enhancement of crystalline perfection by organic dopants in ZTS, ADP and KHP crystals as investigated by high-resolution XRD and SEM [J].

Bhagavannarayana, G. ;

Parthiban, S. ;

Meenakshisundaram, Subbiah .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2006, 39 :784-790

[5] A study of the effect of annealing on Fe-doped LiNbO3 by HRXRD, XRT and FT-IR [J].

Bhagavannarayana, G ;

Ananthamurthy, RV ;

Budakoti, GC ;

Kumar, B ;

Bartwal, KS .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2005, 38 :768-771

[6] Interesting growth features in potassium dihydrogen phosphate: unravelling the origin and dynamics of point defects in single crystals [J].

Bhagavannarayana, G. ;

Rajesh, P. ;

Ramasamy, P. .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2010, 43 :1372-1376

[7] Enhancement of SHG efficiency by urea doping in ZTS single crystals and its correlation with crystalline perfection as revealed by Kurtz powder and high-resolution X-ray diffraction methods [J].

Bhagavannarayana, G. ;

Kushwaha, S. K. .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2010, 43 :154-162

[8] New nonlinear optical material: glycine sodium nitrate [J].

Bhat, MN ;

Dharmaprakash, SM .

JOURNAL OF CRYSTAL GROWTH, 2002, 235 (1-4) :511-516

[9] Synthesis, crystal growth and characterization of L-pyrrolidone-2-carboxylic acid (L-PCA) crystals [J].

Boomadevi, S ;

Dhanasekaran, R .

JOURNAL OF CRYSTAL GROWTH, 2004, 261 (01) :70-76

[10]

Farges J.-P., 1994, ORGANIC CONDUCTORS

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