Identification of odor volatile compounds and deodorization of Paphia undulata enzymatic hydrolysate

被引:26
作者
Chen Deke [1 ,2 ]
Chen Xin [3 ]
Chen Hua [1 ]
Cai Bingna [1 ]
Wan Peng [1 ]
Zhu Xiaolian [1 ,2 ]
Sun Han [4 ]
Sun Huili [1 ]
Pan Jianyu [1 ]
机构
[1] Chinese Acad Sci, Guangdong Key Lab Marine Met Med, Key Lab Trop Marine Bioresource & Ecol, South China Sea Inst Oceanol, Guangzhou 510301, Guangdong, Peoples R China
[2] Univ Chinese Acad Sci, Beijing 100049, Peoples R China
[3] Foshan Univ, Dept Chem & Chem Engn, Foshan 528000, Peoples R China
[4] Rutgers State Univ, 98 Brett Rd, Piscataway, NJ 08854 USA
基金
美国国家科学基金会;
关键词
deodorization; off-flavor; trimethylamine; enzymatic hydrolysate; Paphia undulate; BIOLOGICAL DEODORIZATION; HYDROGEN-SULFIDE; FISH MUSCLE; CHROMATOGRAPHY/MASS SPECTROMETRY; THIOBACILLUS-THIOOXIDANS; PATINOPECTEN-YESSOENSIS; TRIMETHYLAMINE OXIDE; SAMPLE PREPARATION; ACTIVE COMPOUNDS; LIPID OXIDATION;
D O I
10.1007/s11802-016-3166-7
中图分类号
P7 [海洋学];
学科分类号
0707 ;
摘要
Unfavorable fishy odour is an inevitable problem in aquatic products. In the present study, headspace solid-phase microextraction gas chromatography mass spectrometry (HS-SPME-GC-MS) analysis of volatiles from untreated samples and three deodorized samples (under the optimal conditions) of Paphia undulata enzymatic hydrolysate revealed that the compounds contributing to the distinctive odor were 1-octen-3-ol, n-hexanal, n-heptanal, 2,4-heptadienal, and 2,4-decadienal, whereas n-pentanal, n-octanal, n-octanol, benzaldehyde, 2-ethylfuran and 2-pentylfuran were the main contributors to the aromatic flavor. The deodorizing effects of activated carbon (AC) adsorption, yeast extract (YE) masking and tea polyphenol (TP) treatment on a P. undulata enzymatic hydrolysate were investigated using orthogonal experiments with sensory evaluation as the index. The following optimized deodorization conditions were obtained: AC adsorption (35 mg mL(-1), 80A degrees C, 40 min), YE masking (7 mg mL(-1), 45A degrees C, 30 min) and TP treatment (0.4 mg mL(-1), 40A degrees C, 50 min). AC adsorption effectively removed off-flavor volatile aldehydes and ketones. YE masking modified the odor profile by increasing the relative contents of aromatic compounds and decreasing the relative contents of aldehydes and ketones. The TP treatment was not effective in reducing the odor score, but it significantly reduced the relative content of aldehydes while increasing that of alkanes. It is also notable that TP effectively suppressed trimethylamine (TMA) formation in a P. undulate hydrolysate solution for a period of 72 h.
引用
收藏
页码:1101 / 1110
页数:10
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