Solvent-Free, Microwave-Assisted, One-Pot Synthesis of 2-Acetyl-N,3-diaryl-4-nitro-butanamides

被引：3
作者：
Yavari, Issa [1 ]
Beheshti, Saeideh [1 ]
Hossaini, Zinatossadat [1 ]
Souri, Sanaz [1 ]
机构：
[1] Tarbiat Modares Univ, Dept Chem, Tehran, Iran
来源：
SYNTHETIC COMMUNICATIONS | 2011年 / 41卷 / 06期
关键词：
Aniline; butanamide; Michael addition; microwave irradiation; -nitrostyrene; DIRECT CONJUGATE ADDITION; AMINE-THIOUREA CATALYST; BETA-NITROSTYRENES; MICHAEL ADDITIONS; NITROALKENES; ISOCYANIDE; GRIGNARD; REAGENTS; KETONES;
D O I：
10.1080/00397911003707113
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
[image omitted] A microwave-assisted diastereoselective synthesis of 2-acetyl-N,3-diaryl-4-nitro-butanamides via reaction of anilines, 2,2,6-trimethyl-4H-1,3-dioxin-4-one, and -nitrostyrenes in the presence of catalytic amounts of triethylamine under solvent-free conditions is described.
引用
收藏
页码：907 / 913
页数：7
相关论文
共 50 条
  • [41] One-Pot Synthesis of 2,4,5-Triarylimidazoles Catalyzed by Copper (II) Trifluoroacetate Under Solvent-Free Conditions
    Song, Dailei
    Liu, Chunsheng
    Zhang, Shaohua
    Luo, Genxiang
    SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2010, 40 (03) : 145 - 147
  • [42] Microwave-Assisted Synthesis of New Spiro[indoline-3,4'-quinoline] Derivatives via a One-Pot Multicomponent Reaction
    Zhu, Song-Lei
    Zhao, Kai
    Su, Xiao-Ming
    Ji, Shun-Jun
    SYNTHETIC COMMUNICATIONS, 2009, 39 (08) : 1355 - 1366
  • [43] Microwave-assisted, solvent-free, three-component synthesis of 2,4,6-triarylpyridines from benign components
    Zomordbakhsh, Shahab
    Anaraki-Ardakani, Hossein
    Zeeb, Mohsen
    Sadeghi, Mahdi
    Mazraeh-Seffid, Manouchehr
    JOURNAL OF CHEMICAL RESEARCH, 2012, (03) : 138 - 140
  • [44] One-pot preparation of 2-(alkyl)arylbenzoselenazoles from the corresponding N-(acetyl)benzoyl-2-iodoanilines via a microwave-assisted methodology
    Redon, Sebastien
    Kabri, Youssef
    Crozet, Maxime D.
    Vanelle, Patrice
    TETRAHEDRON LETTERS, 2014, 55 (36) : 5052 - 5054
  • [45] Microwave-assisted one-pot synthesis of pyrazolyl-substituted benzochroman-4-one derivatives and evaluation of their anticancer activity
    Ashok, Dongamanti
    Padmavati, Kadiyala
    Lakshmi, Bommidi Vijaya
    Sarasija, Madderla
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2016, 52 (01) : 15 - 20
  • [46] Microwave-assisted one-pot synthesis of pyrazolyl-substituted benzochroman-4-one derivatives and evaluation of their anticancer activity
    Dongamanti Ashok
    Kadiyala Padmavati
    Bommidi Vijaya Lakshmi
    Madderla Sarasija
    Chemistry of Heterocyclic Compounds, 2016, 52 : 15 - 20
  • [47] Microwave Assisted Convenient One-Pot Synthesis of Coumarin Derivatives via Pechmann Condensation Catalyzed by FeF3 under Solvent-Free Conditions and Antimicrobial Activities of the Products
    Vahabi, Vahid
    Hatamjafari, Farhad
    MOLECULES, 2014, 19 (09): : 13093 - 13103
  • [48] SOLVENT-FREE MICROWAVE-ASSISTED PREPARATION OF N-(2-(PYRIDIN-2-YL)-ETHYL) SULFONAMIDES
    Ghattas, Paul
    Carlin, Joseph W.
    Murkli, Steven L., Jr.
    Jacobs, Danielle L.
    SYNTHETIC COMMUNICATIONS, 2014, 44 (04) : 520 - 529
  • [49] One-pot synthesis of 3, 4-dihydropyrimidin-2(1H)-ones catalysed by [BMIM]Br under solvent-free condition
    Rani, J. W. S.
    Kathing, C.
    Singh, N. G.
    Nongrum, R.
    Rahman, N.
    Kharmawlong, G.
    Nongkhlaw, R.
    BULGARIAN CHEMICAL COMMUNICATIONS, 2017, 48 (04): : 3 - 10
  • [50] Microwave-assisted synthesis of new N4-[bi-(4-fluorophenyl)-methyl]-piperazine thiosemicarbazones under solvent-free conditions
    Li, Qing Han
    Zhao, Zhi Gang
    CHINESE CHEMICAL LETTERS, 2008, 19 (09) : 1035 - 1038
12345