Use of semiautomatic equipment for the determination of fumonisin B1 in milk

被引：0

作者：

Scarano, G ^{[1
]}

Grasso, L ^{[1
]}

Arace, O ^{[1
]}

Oliviero, G ^{[1
]}

Serpe, L ^{[1
]}

机构：

[1] Ist Zooprofilatt Sperimentale Mezzogiorno, I-80055 Portici, Na, Italy

来源：

INDUSTRIE ALIMENTARI | 2001年 / 40卷 / 401期

关键词：

D O I：

暂无

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

A HPLC method for the determination of fumonisin in milk was modified. In comparison with the original method, semiautomatic equipment have been used in the purification step by means of immunoaffinity columns, and in the derivatization and LC injection steps. The use of these equipments provided good repeatability, short process time, and in particular the analysis of several samples in the same time could be carried out. The accuracy of the modified method resulted to be acceptable within the considered concentration range. The detector response resulted to be linear in the range 0.001-0.010 mug. The detection limit was 0.010 mug mL(-1). The recovery of fumonisin from milk samples at fortification levels of 0.025, 0.05 and 0.1 mug mL(-1) resulted to be 83.1, 79.7 and 73.5% respectively.

引用

页码：257 / 260

页数：4

共 11 条

[1] Use of automated solid-phase extraction equipment for the determination of isoniazid in milk [J].

Grasso, L ;

Scarano, G ;

Imparato, E ;

Arace, O ;

Oliviero, G .

FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2000, 17 (09) :749-753

[2]

HETIZMANN RJ, VET DRUG RESIDUES RE

[3]

MARAGOS CM, 1994, J AOAC INT, V77, P1162

[4]

Marasas Walter F. O., 1995, Natural Toxins, V3, P193, DOI 10.1002/nt.2620030405

[5]

RILEY RT, 1994, J AOAC INT, V77, P533

[6] A REVIEW AND UPDATE OF ANIMAL TOXICOSES ASSOCIATED WITH FUMONISIN-CONTAMINATED FEEDS AND PRODUCTION OF FUMONISINS BY FUSARIUM ISOLATES [J].

ROSS, PF ;

RICE, LG ;

OSWEILER, GD ;

NELSON, PE ;

RICHARD, JL ;

WILSON, TM .

MYCOPATHOLOGIA, 1992, 117 (1-2) :109-114

[7]

Scarano G, 1998, ANALYST, V123, P2551, DOI 10.1039/a805205k

[8] DETERMINATION OF FUMONISINS IN MILK [J].

SCOTT, PM ;

DELGADO, T ;

PRELUSKY, DB ;

TRENHOLM, HL ;

MILLER, JD .

JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH PART B-PESTICIDES FOOD CONTAMINANTS AND AGRICULTURAL WASTES, 1994, 29 (05) :989-998

[9] Fumonisin B-1-induced sphingolipid depletion inhibits vitamin uptake via the glycosylphosphatidylinositol-anchored folate receptor [J].

Stevens, VL ;

Tang, JH .

JOURNAL OF BIOLOGICAL CHEMISTRY, 1997, 272 (29) :18020-18025

[10] NATURAL OCCURRENCE OF SOME FUSARIUM MYCOTOXINS IN CORN FROM LOW AND HIGH ESOPHAGEAL CANCER PREVALENCE AREAS OF THE TRANSKEI, SOUTHERN AFRICA [J].

SYDENHAM, EW ;

THIEL, PG ;

MARASAS, WFO ;

SHEPHARD, GS ;

VANSCHALKWYK, DJ ;

KOCH, KR .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1990, 38 (10) :1900-1903

← 1 2 →