13C NMR characterization of nanodiamonds

被引：35
|
作者：
Donnet, JB
Fousson, E
Delmotte, L
Samirant, M
Baras, C
Wang, TK
Eckhardt, A
机构：
[1] Ecole Natl Super Chim, Chim Phys Lab, F-68093 Mulhouse, France
[2] Inst Franco Allemad Rech St Louis, F-68301 St Louis, France
[3] Ecole Natl Super Chim, Lab Mat Mineraux, F-68093 Mulhouse, France
[4] Inst Chim Surfaces & Interfaces, F-68057 Mulhouse, France
来源：
COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II FASCICULE C-CHIMIE | 2000年 / 3卷 / 11-12期
关键词：
nanodiamonds; shock compression; detonation; C-13; NMR;
D O I：
10.1016/S1387-1609(00)01208-1
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We have examined by C-13 solid-state NMR crystalline quality of cubic diamond produced either via firing of explosive compositions, or through compression of mixtures containing carbonaceous precursors with metallic matrix. In particular MAS technique was used to estimate sp(3)/sp(2) phases ratios for the obtained condensed carbon, whereas functionality of surface carbon atoms was studied rather via CP-MAS method. (C) 2000 Academie des sciences / Editions scientifiques et medicales Elsevier SAS.
引用
收藏
页码：831 / 838
页数：8
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