Comparative study on cracking behavior of sol-gel silica antireflective coating for high-powered laser system

被引:13
作者
Zhang, Qing-Hua [1 ]
Deng, Xue-Ran [1 ]
Yang, Wei [1 ]
Hui, Hao-Hao [1 ]
Wei, Yao-Wei [1 ]
Chen, Jin-Ju [2 ]
机构
[1] China Acad Engn Phys, Chengdu Fine Opt Engn Res Ctr, Chengdu 610041, Sichuan, Peoples R China
[2] Univ Elect Sci & Technol China, State Key Lab Elect Thin Films & Integrated Devic, Chengdu 610054, Sichuan, Peoples R China
基金
中国国家自然科学基金;
关键词
Cracking behavior; Sol-gel silica antireflective coating; KDP crystal; Residual stress; RESIDUAL-STRESS; RIDGE FORMATION; THIN-FILMS; EXFOLIATION; MECHANISMS; CRYSTALS;
D O I
10.1016/j.engfailanal.2017.08.026
中图分类号
TH [机械、仪表工业];
学科分类号
0802 ;
摘要
Potassium dihydrogen phosphate (KDP) crystal is a kind of very crucial nonlinear optics for highpowered laser equipment as frequency conversion (doubler, tripler or quadrupler) components. In this paper, investigation on cracking behavior of sol-gel silica antireflective (AR) coatings has been performed using KDP crystal as substrate. Cracking induced by heating or moisturizing posttreatment is respectively studied, in which distinct cracking behaviors have been observed. It has been interestingly found that either temperature or humidity saltation can result in coating crack generation, but the corresponding residual stress demonstrates in completely reverse ways, giving rise to distinctive crack morphology on both crack edge and bottom. The origination and the derivation of such stress manner have been stated based on the intrinsic porous structure of sol-gel silica coating, and the critical cracking condition has been suggested dependent on the relationship between the accumulated residual stress against elastic recovery capability of such coating.
引用
收藏
页码:64 / 71
页数:8
相关论文
共 22 条
[1]   THERMAL EXPANSION OF CRYSTALS WITH KH2PO4 STRUCTURE [J].
COOK, WR .
JOURNAL OF APPLIED PHYSICS, 1967, 38 (04) :1637-&
[2]   Effect of Poly(vinylpyrrolidone) As a Stress-Relaxing Additive in Fabrication of PbZrxTi1-xO3 Thin Films Using Sol-Gel Route [J].
Doi, Toshihiro ;
Soyama, Nobuyuki ;
Sakurai, Hideaki .
JAPANESE JOURNAL OF APPLIED PHYSICS, 2013, 52 (09)
[3]   MECHANISMS OF HYDROGEN INDUCED DELAYED CRACKING IN HYDRIDE FORMING MATERIALS [J].
DUTTON, R ;
NUTTALL, K ;
PULS, MP ;
SIMPSON, LA .
METALLURGICAL TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1977, 8 (10) :1553-1562
[4]  
Fang T, 2002, J AM CERAM SOC, V85, P174, DOI 10.1111/j.1151-2916.2002.tb00062.x
[5]   Multiple cracking of thin films due to residual stress combined with bending stress [J].
Fu, Y. ;
Zhang, X. C. ;
Xuan, F. Z. ;
Tu, S. T. ;
Wang, Z. D. .
COMPUTATIONAL MATERIALS SCIENCE, 2013, 73 :113-119
[6]   Residual stress and cracking in expanded austenite layers [J].
Hoeft, D ;
Latella, BA ;
Short, KT .
JOURNAL OF PHYSICS-CONDENSED MATTER, 2005, 17 (23) :3547-3558
[7]   A surface-emitting laser incorporating a high-index-contrast subwavelength grating [J].
Huang, Michael C. Y. ;
Zhou, Y. ;
Chang-Hasnain, Connie J. .
NATURE PHOTONICS, 2007, 1 (02) :119-122
[8]   Effects of stress ratio on fatigue crack propagation properties of submicron-thick free-standing copper films [J].
Kondo, Toshiyuki ;
Imaoka, Takahiro ;
Hirakata, Hiroyuki ;
Sakihara, Masayuki ;
Minoshima, Kohji .
ACTA MATERIALIA, 2013, 61 (16) :6310-6327
[9]   Mechanical response of KD2xH2(1-x)PO4 crystals during nanoindentation [J].
Kucheyev, SO ;
Siekhaus, WJ ;
Land, TA ;
Demos, SG .
APPLIED PHYSICS LETTERS, 2004, 84 (13) :2274-2276
[10]   Mechanical properties of hybrid organic-inorganic materials [J].
Mammeri, F ;
Le Bourhis, E ;
Rozes, L ;
Sanchez, C .
JOURNAL OF MATERIALS CHEMISTRY, 2005, 15 (35-36) :3787-3811