Crystal growth and characterization of semiorganic single crystals of L-histidine family for NLO applications

被引：30

作者：

Anandan, Pandurangan ^{[1
,2
]}

Jayavel, Ramasamy ^{[1
]}

机构：

[1] Anna Univ, Ctr Crystal Growth, Madras 600025, Tamil Nadu, India

[2] Thiruvalluvar Coll Engn & Technol, Dept Phys, Vandhavasi 604505, India

来源：

JOURNAL OF CRYSTAL GROWTH | 2011年 / 322卷 / 01期

关键词：

X-ray diffraction; Thermal analysis; Solution growth; Semiorganic; NONLINEAR-OPTICAL CRYSTAL; L-ARGININE PHOSPHATE; HYDROCHLORIDE MONOHYDRATE; BROMIDE; SPECTRA;

D O I：

10.1016/j.jcrysgro.2011.02.021

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Single crystals of L-histidine hydrochloride monohydrate and tartaric acid mixed L-histidine hydrochloride monohydrate have been grown by slow evaporation solution growth technique from appropriate mixtures of respective chemicals. Single crystal and powder X-ray diffraction analyses, Fourier transform infrared, nuclear magnetic resonance spectral analysis, thermo-gravimetric (TG), differential thermal analysis (DTA) have been employed to characterize the as-grown crystals. It is observed to be a wide transparency window for both the crystals from 300 to 1000 nm, which is suitable for second harmonic generation of laser in the blue region. Nonlinear optical characteristics have been studied using Q switched Nd:YAG laser (lambda=1064 nm). The second harmonic generation conversion efficiency of the grown crystal shows the suitability for frequency conversion applications. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：69 / 73

页数：5

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