Complete 1H and 13C NMR assignments of two new trans-clerodane diterpenoids from Otostegia limbata

被引:3
作者
Farooq, Umar
Khan, Afsar
Ahmad, Viqar Uddin [1 ]
Azhar-Ul-Haq
Khan, Saleha Suleman
Farooq, Robina
Pervez, Arshid
Shah, Mohammad Mahroof
机构
[1] Univ Karachi, HEJ Res Inst Chem, Int Ctr Chem & Biol Sci, Karachi 75270, Pakistan
[2] COMSATS Inst Informat Technol, Dept Environm Sci, Abbottabad, Pakistan
关键词
NMR; 1D/2D NMR; ballotenic acid A; ballodiolic acid A; trans-clerodane; tricyclic diterpenoids; Otostegia limbata; lamiaceae;
D O I
10.1002/mrc.2047
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Two new tricyclic trans-clerodane diterpenoids trivially named as ballotenic acid A (1) and ballodiolic acid A (2) have been isolated from ethyl acetate fraction of Otostegia limbata. The structure assignments are based on H-1 and C-13 NMR spectra, 2D NMR (HMQC, HMBC, COSY, NOESY and NOE) techniques and comparison with the literature data. Copyright (C) 2007 John Wiley & Sons, Ltd.
引用
收藏
页码:766 / 769
页数:4
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