Preparation of mesoporous petal-like MgAl2O4 via molten-salt assisted nonhydrolytic sol-gel method

被引:3
作者
Wu, Qian [1 ,2 ]
Feng, Guo [2 ]
Miao, Lifeng [2 ]
Tang, Zijuan [1 ]
Jiang, Weihui [1 ,2 ]
Liang, Jian [2 ]
Liu, Jianmin [2 ]
机构
[1] Jingdezhen Ceram Inst, Dept Mat Sci & Engn, Jingdezhen 333000, Peoples R China
[2] Jingdezhen Ceram Inst, Natl Engn Res Ctr Domest & Bldg Ceram, Jingdezhen 333000, Peoples R China
基金
中国国家自然科学基金;
关键词
MgAl2O4; Petal-like; Mesoporous; Nonhydrolytic sol-gel method; Molten-salt method; SPINEL; CATALYSTS; MECHANISM; NANORODS; PROPANE; POWDER; CARBON;
D O I
10.1016/j.cplett.2021.138794
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Mesoporous petal-like MgAl2O4 spinel has been prepared by molten salt assisted nonhydrolytic sol-gel method. The influence of Mg/Al molar ratio (0.45, 0.50, 0.55, 0.60, 0.70 and 0.80) on the morphology and surface area of MgAl2O4 was investigated. The results reveal that Mg/Al molar ratio has a significant influence on the morphology. At Mg/Al molar ratio of 0.7, the achieved petal-like MgAl2O4 is highly uniformed in morphology, the surface area and pore volume reached maximum values of 141 m(2)g(-1) and 0.24 cm(3)g(-1), respectively. These properties make it have promising applications in the catalyst support field.
引用
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页数:7
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