High pressure Raman spectra of DL-lysine hydrochloride

被引：2
作者：
Batista, J. C. [1 ,2 ]
Lima, J. A., Jr. [1 ]
Freire, P. T. C. [1 ]
Melo, F. E. A. [1 ]
Mendes-Filho, J. [1 ]
机构：
[1] Univ Fed Ceara, Dept Fis, CP 6030,Campus Pici, BR-60455760 Fortaleza, Ceara, Brazil
[2] Inst Fed Educ Ciencia & Tecnol Piaui, BR-64605500 Picos, PI, Brazil
来源：
VIBRATIONAL SPECTROSCOPY | 2016年 / 86卷
关键词：
L-lysine hydrochloride; Amino acid; High-pressure; Phase transition; Raman spectroscopy; INDUCED PHASE-TRANSITIONS; X-RAY-DIFFRACTION; MONOHYDRATED L-ASPARAGINE; DIAMOND-ANVIL CELL; L-ALANINE; MONOHYDROCHLORIDE DIHYDRATE; AMINO-ACIDS; L-VALINE; CRYSTAL; SPECTROSCOPY;
D O I：
10.1016/j.vibspec.2016.08.011
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
DL-lysine hydrochloride crystals were studied by Raman spectroscopy under hydrostatic pressure using a diamond anvil cell from ambient pressure up to 9.8 GPa in the spectral range from 1150 to 40 cm(-1). Changes in the Raman spectrum were observed in all spectral regions analyzed. In particular, modifications in the lattice modes indicate that the crystal undergoes a phase transition. The classification of the vibrational modes, the behavior of their band wavenumber as a function of the pressure and the reversibility of the phase transitions are also discussed. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码：337 / 342
页数：6
相关论文
共 39 条
  • [1] High pressure Raman scattering of DL-leucine crystals
    Abagaro, B. T. O.
    Freire, P. T. C.
    Silva, J. G.
    Melo, F. E. A.
    Lima, J. A., Jr.
    Mendes Filho, J.
    Pizani, P. S.
    [J]. VIBRATIONAL SPECTROSCOPY, 2013, 66 : 119 - 122
  • [2] OPTICAL FLUORESCENCE SYSTEM FOR QUANTITATIVE PRESSURE MEASUREMENT IN DIAMOND-ANVIL CELL
    BARNETT, JD
    BLOCK, S
    PIERMARINI, GJ
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1973, 44 (01) : 1 - 9
  • [3] CRYSTAL AND MOLECULAR-STRUCTURE OF DL-LYSINE HYDROCHLORIDE
    BHADURI, D
    SAHA, NN
    [J]. JOURNAL OF CRYSTAL AND MOLECULAR STRUCTURE, 1979, 9 (06): : 311 - 316
  • [4] A comparative study of the anisotropy of lattice strain induced in the crystals of L-serine by cooling down to 100 K or by increasing pressure up to 4.4 GPa
    Boldyreva, EV
    Kolesnik, EN
    Drebushchak, TN
    Ahsbahs, H
    Beukes, JA
    Weber, HP
    [J]. ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2005, 220 (01): : 58 - 65
  • [5] Effect of high pressure on crystalline glycine: A new high-pressure polymorph
    Boldyreva, EV
    Ivashevskaya, SN
    Sowa, H
    Ahsbahs, H
    Weber, HP
    [J]. DOKLADY PHYSICAL CHEMISTRY, 2004, 396 (1-3) : 111 - 114
  • [6] Effect of hydrostatic pressure on the γ-polymorph of glycine -: 1.: A polymorphic transition into a new δ-form
    Boldyreva, EV
    Ivashevskaya, SN
    Sowa, H
    Ahsbahs, H
    Weber, HP
    [J]. ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2005, 220 (01): : 50 - 57
  • [7] Different dynamics of chiral and racemic (L- and DL-) serine crystals: Evidenced by incoherent inelastic neutron and Raman scattering
    Bordallo, Heloisa N.
    Kolesov, Boris A.
    Boldyreva, Elena V.
    Juranyi, Fanni
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2007, 129 (36) : 10984 - +
  • [8] Solid-Solid Phase Transitions in DL-Norvaline Studied by Differential Scanning Calorimetry and Raman Spectroscopy
    Chatzigeorgiou, Petros
    Papakonstantopoulos, Nikos
    Tagaroulia, Nikolitsa
    Pollatos, Evangelos
    Xynogalas, Pantelis
    Viras, Kyriakos
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2010, 114 (03) : 1294 - 1300
  • [9] A DIAMOND-ANVIL CELL FOR IR MICROSPECTROSCOPY
    CHERVIN, JC
    CANNY, B
    BESSON, JM
    PRUZAN, P
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (03) : 2595 - 2598
  • [10] The Elusive High Temperature Solid-State Structure of D,L-Norleucine
    Coles, S. J.
    Gelbrich, T.
    Griesser, U. J.
    Hursthouse, M. B.
    Pitak, M.
    Threlfall, T.
    [J]. CRYSTAL GROWTH & DESIGN, 2009, 9 (11) : 4610 - 4612
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