The 1:1 proton-transfer compound of sulfanilamide with 3,5-dinitrosalicylic acid

被引:15
作者
Smith, G
Wermuth, UD
White, JM
机构
[1] Queensland Univ Technol, Ctr Instrumental & Dev Chem, Brisbane, Qld 4001, Australia
[2] Univ Melbourne, Sch Chem, Parkville, Vic 3052, Australia
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2001年 / 57卷
关键词
D O I
10.1107/S1600536801016841
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the proton-transfer compound from the reaction of 3,5-dinitrosalicylic acid (DNSA) with sulfanilamide (ABSA), i.e. 4-sulfonamidoanilinium 3,5-dinitrosalicylate, C6H9N2O2S+.C7H3N2O7-, shows an extensively hydrogen-bonded polymeric structure in which the protonated amino group of sulfanilamide together with the amide group give a total of eight intermolecular interactions with most of the O atoms of the DNSA anions [N . . .O 2.822 (2)-3.172 (2) Angstrom], together with both of the sulfonate O atoms of adjacent ABSA cations [N . . .O 2.867 (2) and 3.090 (2) Angstrom].
引用
收藏
页码:O1036 / O1038
页数:3
相关论文
共 13 条
[1]  
Enraf-Nonius, 1989, CAD 4 SOFTW VERS 5 0
[2]  
GABLE RW, 1994, PROCESS DATA
[3]  
Kumar VSS, 1999, J CHEM SOC PERK T 2, P1069
[4]  
Sheldrick G.M., 1997, SHELXS PROGRAM CRYST
[5]  
Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S0108767307043930]
[6]   Molecular co-crystals of carboxylic acids .23. The 1:1 adducts of 3-amino-1H-1,2,4-triazole with 5-nitrosalicylic acid and 3,5-dinitrosalicylic acid [J].
Smith, G ;
Lynch, DE ;
Byriel, KA ;
Kennard, CHL .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 :231-235
[7]   MOLECULAR COCRYSTALS OF CARBOXYLIC-ACIDS .20. THE CRYSTAL-STRUCTURES OF 3,5-DINITROSALICYLIC ACID AND ITS ADDUCTS WITH THE ISOMERIC MONOAMINOBENZOIC ACIDS [J].
SMITH, G ;
LYNCH, DE ;
BYRIEL, KA ;
KENNARD, CHL .
AUSTRALIAN JOURNAL OF CHEMISTRY, 1995, 48 (06) :1133-1149
[8]   Interactions of aromatic carboxylic acids with quinolin-8-ol (oxine): synthesis and the crystal structures of the proton-transfer compounds with the nitro-substituted benzoic acids [J].
Smith, G ;
Wermuth, UD ;
White, JM .
AUSTRALIAN JOURNAL OF CHEMISTRY, 2001, 54 (03) :171-175
[9]   Interactions of aromatic carboxylic acids with 8-aminoquinoline: Synthesis and the crystal structures of the proton-transfer compounds of 8-aminoquinoline with nitro-substituted benzoic acids [J].
Smith, G ;
Wermuth, UD ;
Bott, RC ;
White, JM ;
Willis, AC .
AUSTRALIAN JOURNAL OF CHEMISTRY, 2001, 54 (03) :165-170
[10]   Guanidinium 3,5-dinitrosalicylate [J].
Smith, G ;
Bott, RC ;
Wermuth, UD .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 :o640-o642