Crystal structure of 4,7-dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene

被引：0

作者：

Deng, Shun-Liu ^{[1
]}

Li, Sa ^{[1
]}

Huang, Rong-Bin ^{[1
]}

Zheng, Lan-Sun ^{[1
,2
]}

机构：

[1] Xiamen Univ, Coll Chem & Chem Engn, Dept Chem, Xiamen 361005, Peoples R China

[2] Xiamen Univ, Key Lab Phys Chem Solid Surfaces, Xiamen 361005, Peoples R China

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2008年 / 38卷 / 09期

基金：

中国国家自然科学基金;

关键词：

acenaphthylene; X-ray crystallography; C-H center dot center dot center dot O interaction;

D O I：

10.1007/s10870-008-9373-3

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound was prepared from the reaction of perchloroacenaphthylene with an excess of sodium salt of 4-methyloxythiophenol in toluene/ethanol (1:1) solvent and structurally characterized by single-crystal X-ray diffraction. The compound crystallizes in the Monoclinic space group P2(1) with the parameters: a = 10.351(1) angstrom, b = 20.453(3) angstrom, c = 12.1837(16) angstrom, beta = 105.584(3)degrees, V = 2484.5(6) angstrom(3), with Z = 2 formula units.

引用

页码：679 / 683

页数：5

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