Crystal structure of 4,7-dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene

被引：0
作者：
Deng, Shun-Liu [1 ]
Li, Sa [1 ]
Huang, Rong-Bin [1 ]
Zheng, Lan-Sun [1 ,2 ]
机构：
[1] Xiamen Univ, Coll Chem & Chem Engn, Dept Chem, Xiamen 361005, Peoples R China
[2] Xiamen Univ, Key Lab Phys Chem Solid Surfaces, Xiamen 361005, Peoples R China
来源：
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2008年 / 38卷 / 09期
基金：
中国国家自然科学基金;
关键词：
acenaphthylene; X-ray crystallography; C-H center dot center dot center dot O interaction;
D O I：
10.1007/s10870-008-9373-3
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound was prepared from the reaction of perchloroacenaphthylene with an excess of sodium salt of 4-methyloxythiophenol in toluene/ethanol (1:1) solvent and structurally characterized by single-crystal X-ray diffraction. The compound crystallizes in the Monoclinic space group P2(1) with the parameters: a = 10.351(1) angstrom, b = 20.453(3) angstrom, c = 12.1837(16) angstrom, beta = 105.584(3)degrees, V = 2484.5(6) angstrom(3), with Z = 2 formula units.
引用
收藏
页码：679 / 683
页数：5
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