{4-[(2,4-Dichlorobenzoyloxy)methyl]-1-phenyl-1H-1,2,3-triazol-5-yl}methyl 2,4-dichlorobenzoate

被引：0

作者：

Ismatov, Dilmurot ^{[1
]}

Azizov, Umarkhon ^{[2
]}

Talipov, Samat ^{[3
]}

Ashurov, Jamshid ^{[3
]}

机构：

[1] Tashkent Chem Technol Inst, Tashkent, Uzbekistan

[2] Uzbekistan Sci Res Pharmacol Chem Inst, Durmon Yuli 40, Uzbekistan

[3] Acad Sci Uzbek, Inst Bioorgan Chem, Tashkent 100125, Uzbekistan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

data-to-parameter ratio = 13.2; mean σ(C-C) = 0.003 Å; R factor = 0.037; single-crystal X-ray study; T = 293 K; wR factor = 0.107;

D O I：

10.1107/S1600536811035550

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title molecule, C24H15Cl4N3O4, the triazole ring makes dihedral angles of 72.02 (12), 81.60 (12) and 73.82 (11)degrees, respectively, with the adjacent phenyl ring and the two dichlorobenzene rings. In the crystal, a weak C-H center dot center dot center dot N interaction, a short Cl center dot center dot center dot Cl contact [3.307 (2) angstrom] and a pi-pi stacking interaction [centroid-centroid distance = 3.568 (4) angstrom] are observed. An intramolecular C-H center dot center dot center dot O interaction is also present.

引用

页码：O2590 / U2003

页数：10

共 7 条

[1] [Anonymous], XP
[2] DZHURAYEV AD, 1990, KHIM FARM ZH+, V24, P30
[3] Diethyl 3,8-dimethyl-4,7-diazadeca-2,8-dienedioate
Jin, ZM
Li, L
Li, MC
Hu, ML
Shen, L
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 : O642 - O643
[4] KARIMKULOV KM, 1991, KHIM FARM ZH+, V25, P40
[5] Oxford Diffraction, 2009, CRYSALIS PRO
[6] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
[7] Zakirov A U, 2001, Eksp Klin Farmakol, V64, P50

← 1 →