An efficient and green synthesis of 5-oxo-5, 6, 7, 8-tetrahydro-4H-benzo-[b]-pyran derivatives promoted by InCl3•4H2O under microwave irradiation

被引:0
作者
Hu, XY
Fan, XS [1 ]
Zhang, XY
Qu, GR
Li, YZ
机构
[1] Henan Normal Univ, Sch Chem & Environm Sci, Henan Key Lab Environm Pollut Control, Xinxiang 453007, Peoples R China
[2] Chongqing Univ Med Sci, Chongqing 400016, Peoples R China
关键词
pyran derivatives; indium trichloride; microwave irradiation;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A rapid and facile preparation of benzo-[b]-pyran derivatives through condensation of chalcone and 5, 5-dimethyl-1,3-cyclohexandione under microwave irradiation in the presence of catalytic amount of InCl(3 center dot)4H(2)O has been developed. With its high efficiency, operational simplicity and environmental benignancy, this method may provide a useful alternative for the preparation of benzo-[b]-pyran derivatives.
引用
收藏
页码:886 / 888
页数:3
相关论文
共 50 条
[31]   Synthesis of novel 6,6a,7,8-tetrahydro-5H-naphtho[1,2-e]pyrimido[4,5-b][1,4]diazepines under microwave irradiation as potential anti-tumor agents [J].
Insuasty, Braulio ;
Garcia, Angelica ;
Quiroga, Jairo ;
Abonia, Rodrigo ;
Nogueras, Manuel ;
Cobo, Justo .
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2010, 45 (07) :2841-2846
[32]   Synthesis of novel 6-amino-2-(hydroxymethyl)-8-aryl-7-(phenylsulfonyl)pyrano[3,2-b]pyran-4(8H)-one derivatives catalyzed by nano-cellulose-OSO3H [J].
Bahareh Sadeghi .
Research on Chemical Intermediates, 2019, 45 :4897-4906
[33]   Synthesis of novel 6-amino-2-(hydroxymethyl)-8-aryl-7-(phenylsulfonyl)pyrano[3,2-b]pyran-4(8H)-one derivatives catalyzed by nano-cellulose-OSO3H [J].
Sadeghi, Bahareh .
RESEARCH ON CHEMICAL INTERMEDIATES, 2019, 45 (10) :4897-4906
[34]   Synthesis and Crystal Structure of 3,7,7-Trimethyl-1-phenyl-4-(3-nitrophenyl)-4,5,6,7,8,9-hexahydro-1H-pyrazolo[3,4-b]quinoline-5(6H)-one [J].
XU Jia-Ning TU Shu-Jiang② JIANG Hong ZHANG Jin-Peng ZHU Xiao-Tong WANG Qian(Department of Chemistry .
Chinese Journal of Structural Chemistry, 2005, (02) :209-213
[35]   Synthesis and crystal structure of 3,7,7-trimethyl-1-phenyl-4-(3-nitrophenyl)-4,5,6,7,8,9-hexahydro-1H-pyrazolo [3,4-b]quinoline-5(6H)-one [J].
Xu, JN ;
Tu, SJ ;
Jiang, H ;
Zhang, JP ;
Zhu, XT ;
Wang, Q .
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2005, 24 (02) :209-213
[36]   Synthesis and Crystal Structure of 4-(2- Chlorophenyl)-5-cyano-3-methyl-6-oxo-1- phenyl-4,5,6,7-tetrahydropyrazolo[3,4-b] Pyridine under Microwave Irradiation [J].
ZHU SongLeia b TU ShuJianga LI TuanJiea ZOU Xianga ZHANG XiaoJinga JI ShunJunc ZHANG Yongc a Department of Chemistry Xuzhou Normal University Key Laboratory of Biotechnology on Medical Plant Xuzhou Jiangsu China bDepartment of Chemistry Xuzhou Medical College Xuzhou Jiangsu China c College of Chemistry and Chemical Engineering Key Lab of Org Synth of Jiangsu Province Suzhou University Suzhou Jiangsu China .
结构化学, 2004, (11) :1222-1225
[37]   Highly active magnetically separable CuFe2O4 nanocatalyst: an efficient catalyst for the green synthesis of tetrahydrofuro[3,4-b]quinoline-1,8(3H,4H) dione derivatives [J].
Ghahremanzadeh, Ramin ;
Rashid, Zahra ;
Zarnani, Amir-Hassan ;
Naeimi, Hossein .
JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2014, 11 (05) :1407-1419
[38]   New potential biologically active compounds:: Design and an efficient synthesis of N-substituted 4-aryl-4,6,7,8-tetrahydroquinoline-2,5(1H,3H)-diones under microwave irradiation [J].
Tu, SJ ;
Zhu, XT ;
Zhang, JP ;
Xu, JN ;
Zhang, Y ;
Wang, Q ;
Jia, RH ;
Jiang, B ;
Zhang, JY ;
Yao, CS .
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2006, 16 (11) :2925-2928
[39]   Synthesis of Phenyl-substituted 2H,5H-Pyrano[4,3-b]pyran-5-ones and Related Heterocycles via a Domino Knoevenagel Condensation/6π-Electron Electrocyclization of 4-Hydroxy-6-phenyl-2H-pyran-2-one with Cyclic and Acyclic α,β-Unsaturated Aldehydes under Different Conditions [J].
Leutbecher, Heiko ;
Rieg, Sylvia ;
Conrad, Juergen ;
Mika, Sabine ;
Klaiber, Iris ;
Beifuss, Uwe .
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 2009, 64 (08) :935-944
[40]   Synthesis of 4-aryl-3-methyl-6-oxo-4,5,6,7-tetrahydro-2H-pyrazolo[3,4-b]pyridine-5-carbonitrile via a one-pot, three-component reaction [J].
Rahmati, Abbas .
TETRAHEDRON LETTERS, 2010, 51 (22) :2967-2970