Hydrogen evolution assisted deposition of a three-dimensional porous nickel film for the electrocatalytic oxidation of histamine

被引:14
作者
Wang, Jia [1 ]
Liu, Yuan [1 ]
Deng, Xiling [1 ]
Zhao, Na [1 ]
Ying, Xue [1 ]
Ye, Bang-Ce [3 ]
Li, Yingchun [2 ]
机构
[1] Shihezi Univ, Sch Pharm, Key Lab Xinjiang Phytomed Resources, Minist Educ, Shihezi 832000, Peoples R China
[2] Harbin Inst Technol, Coll Sci, Shenzhen 518055, Peoples R China
[3] Shihezi Univ, Sch Chem & Chem Engn, Key Lab Green Proc Chem Engn Xinjiang Bingtuan, Shihezi 832003, Peoples R China
基金
中国国家自然科学基金;
关键词
Electrochemical sensor; Microporous nickel; Galvanostatic deposition; Cyclic voltammetry; Scanning electron microscopy; Energy dispersive spectrometry; X-ray hotoelectron spectroscopy; Trace determination; Fish analysis; GLASSY-CARBON ELECTRODE; ELECTROCHEMICAL DETERMINATION; AMPEROMETRIC DETECTION; GRAPHENE; NANOPARTICLES; PERFORMANCE; DOPAMINE; OXIDE;
D O I
10.1007/s00604-017-2411-0
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The authors describe an electrochemical sensor for ultrasensitive voltammetric of histamine (HA) by using a gold electrode that was modified with a film consisting of threedimensional activated microporous nickel (AMPNi/GE). The porous nickel film was deposited on the electrode by hydrogen evolution assisted electrodeposition. The sensor was characterized via scanning electron microscopy, energy dispersive spectrometry, X-ray photoelectron spectroscopy and cyclic voltammetry in order to evaluate its morphology, composition and electrochemical properties. The pore size and wall thickness of the nickel skeleton were tailored by optimizing the concentration of the plating solution, operating temperature, and deposition time. Under the optimum conditions and in 0.1 M NaOH solution at a typical potential of 0.63 V (vs. Ag/AgCl) at a scan rate of 100 mV s(-1,) the sensor gives an analytical response over the 10 nM to 80 mu M HA concentration range, with a 4.2 nM detection limit (S/N = 3) and a 2.38 mu A.mu M-1.cm(-2) sensitivity. The method is sensitive, repeatable, and the sensor is stable.
引用
收藏
页码:3893 / 3900
页数:8
相关论文
共 50 条
  • [21] Efficient hydrogen evolution electrocatalysts from LixMoS2 nanoparticles on three-dimensional substrate
    Yang, Qiangbin
    He, Yi
    Fan, Yi
    Chen, Xi
    Li, Yubin
    [J]. INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2017, 42 (10) : 6482 - 6489
  • [22] A three-dimensional electrode fabricated by electrophoretic deposition of graphene on nickel foam for structural supercapacitors
    Wang, Juan
    Xu, Chang
    Zhang, Dong
    [J]. NEW JOURNAL OF CHEMISTRY, 2021, 45 (39) : 18567 - 18574
  • [23] In Situ Preparation of Three-Dimensional Porous Nickel Sulfide as a Battery-Type Supercapacitor
    Xia, Qixun
    Si, Lijun
    Liu, Keke
    Zhou, Aiguo
    Su, Chen
    Shinde, Nanasaheb M.
    Fan, Guangxin
    Dou, Jun
    [J]. MOLECULES, 2023, 28 (11):
  • [24] Fabrication and High Electrocatalytic Activity of Three-Dimensional Porous Nanosheet Pt/Boron-Doped Diamond Hybrid Film
    Tong, Xili
    Zhao, Guohua
    Liu, Meichuan
    Cao, Tongcheng
    Liu, Lei
    Li, Peiqiang
    [J]. JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 113 (31) : 13787 - 13792
  • [25] Nickel cobalt phosphide with three-dimensional nanostructure as a highly efficient electrocatalyst for hydrogen evolution reaction in both acidic and alkaline electrolytes
    Ma, Bo
    Yang, Zhengchun
    Chen, Yantao
    Yuan, Zhihao
    [J]. NANO RESEARCH, 2019, 12 (02) : 375 - 380
  • [26] Impact of Iron in Three-Dimensional Co-MOF for Electrocatalytic Water Oxidation
    Sahoo, Malaya K.
    Samantara, Aneeya K.
    Behera, J. N.
    [J]. INORGANIC CHEMISTRY, 2022, 61 (01) : 62 - 72
  • [27] Three-Dimensional Macroscopic Assemblies of Low-Dimensional Carbon Nitrides for Enhanced Hydrogen Evolution
    Jun, Young-Si
    Park, Jihee
    Lee, Sun Uk
    Thomas, Arne
    Hong, Won Hi
    Stucky, Galen D.
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2013, 52 (42) : 11083 - 11087
  • [28] Three-Dimensional PdCuRu Alloy Porous Nanosheets as Efficient Electrocatalysts for Hydrogen Evolution Reaction in Varied Electrolytes
    Yuan, Mengyu
    Xu, Hui
    Wang, Yuan
    Jin, Liujun
    Wang, Cheng
    Chen, Chunyan
    Wang, Yong
    Shang, Hongyuan
    Du, Yukou
    [J]. CHEMELECTROCHEM, 2020, 7 (14): : 3135 - 3139
  • [29] Investigation on the electrocatalytic activity and stability of three-dimensional and two-dimensional palladium nanostructures for ethanol and formic acid oxidation
    Yazdan-Abad, Mehdi Zareie
    Noroozifar, Meissam
    Alfi, Nafiseh
    [J]. JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2018, 532 : 485 - 490
  • [30] Prickly Pear-Like Three-Dimensional Porous MoS2: Synthesis, Characterization and Advanced Hydrogen Evolution Reaction
    Lu, Huiting
    Chen, Xin
    Dai, Wenhao
    Zhang, Kai
    Liu, Conghui
    Dong, Haifeng
    [J]. CATALYSTS, 2018, 8 (06):