Syntheses of MO2 (M = Si, Ce, Sn) nanoparticles by solid-state reactions at ambient temperature

被引:107
作者
Li, F
Yu, XH
Pan, HJ
Wang, ML
Xin, XQ [1 ]
机构
[1] Nanjing Univ, State Key Lab Coordinat Chem, Dept Chem, Nanjing 210093, Peoples R China
[2] Univ Tennessee, Dept Chem, Knoxville, TN 37996 USA
基金
中国国家自然科学基金;
关键词
SiO2; CeO2; SnO2; synthesis; nanoparticles; solid-state reactions;
D O I
10.1016/S1293-2558(00)01084-0
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Nano oxides (SiO2, CeO2, SnO2) were successfully synthesized by solid-state reactions at ambient temperature. The nanoparticles were characterized by X-ray powder diffraction, TEM, BET, and TGA-DTA. The SiO2 particles were also investigated using IR spectra. Effects of calcination on the nanoparticles were studied in this paper. The solid-state reaction technique is a convenient, inexpensive and an effective preparation method of monodisperse oxide nanoparticles in high yield. The mechanisms of the formation of nano materials by solid-state reactions at ambient temperature were primarily investigated. (C) 2000 Editions scientifiques et medicales Elsevier SAS. All rights reserved.
引用
收藏
页码:767 / 772
页数:6
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