Response surface methodology for the microwave-assisted extraction of insecticides from soil samples

被引：24
|
作者：
Hernandez-Soriano, M. Carmen [1 ]
Pena, Aranzazu [1 ]
Mingorance, M. Dolores [1 ]
机构：
[1] CSIC, Dept Ciencias Tierra & Quim Ambiental, Estac Expt Zaidin, E-18008 Granada, Spain
来源：
ANALYTICAL AND BIOANALYTICAL CHEMISTRY | 2007年 / 389卷 / 02期
关键词：
microwave-assisted extraction; soil samples; pyrethroid pesticides; organophosphorous pesticides; Box-Behnken design; desirability function;
D O I：
10.1007/s00216-007-1418-5
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
The extraction of two pyrethroid insecticides (deltamethrin and alpha-cypermethrin) together with three organophosphorus insecticides (dimethoate, diazinon and malathion) from soil samples was carried out with microwave-assisted technology. Experimental designs showed that extraction temperature, addition of water to the extractant and solvent/soil ratio were the variables that affected the recoveries of the pesticide the most. Response surface methodology was applied to find the optimum values of the variables involved in the extractions of the analytes. In addition, in order to achieve near-optimal extraction conditions, a desirability function was used to optimize the five pesticides simultaneously. The optimized conditions were applied to different types of soils.
引用
收藏
页码：619 / 630
页数：12
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