A facile method for preparing VO2 nanobelts

被引:78
|
作者
Liu, Xinghai [1 ]
Xie, Guangyong [2 ,3 ]
Huang, Chi [1 ]
Xu, Qian [1 ]
Zhang, Yifu [1 ]
Luo, Yunbai [1 ]
机构
[1] Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China
[2] S Cent Univ Nationalities, Coll Chem & Mat Sci, Key Lab Catalysis & Mat Sci, State Ethn Affairs Commiss, Wuhan 430074, Peoples R China
[3] S Cent Univ Nationalities, Minist Educ, Coll Chem & Mat Sci, Wuhan 430074, Peoples R China
关键词
nanomaterials; VO2; nanobelts; hydrothermal; x-ray diffraction;
D O I
10.1016/j.matlet.2007.10.022
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Metastable VO2 nanobelts were synthesized via a facile hydrothermal approach. Then the as-obtained samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). Typical samples exhibited monoclinic phase VO2 (B) indexed as XRD, and the XPS results demonstrated that the V (IV) existed only in vanadium oxides. According to the results of TEM and SEM, the VO2 (B) nanobelts were 0.6-2.2 mu m long, typically 70-180 nm wide and 20-30 nm thick. Some factors that affected the shape of One-dimensional (1-D) VO2 nanomaterials were briefly discussed. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:1878 / 1880
页数:3
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