Determination of esters in motor and industrial oils by IR spectrometry

被引:5
作者
Gol'eva, VE
Rudnev, MI
Pisanov, VA
机构
[1] Rostov State Univ, Dept Chem, Rostov Na Donu 344090, Russia
[2] S Customs Agcy, Expert Criminalist Serv, Rostov Na Donu 344011, Russia
关键词
Ester; Analytical Chemistry; Absorption Band; Isopropyl; Band Intensity;
D O I
10.1007/s10809-005-0169-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
IR spectra of mixtures of mineral oil and isopropyl myristate modeling motor oils with different concentrations of esters were studied. A relationship between the absorption band intensities at 1737, 1180, and 1110 cm(-1) and the ester concentration in the oil was revealed. A procedure was proposed for the determination of esters in motor oils by IR spectrometry (c(min) = 1%; RSD <= 8.6%). The procedure was tested on several commercially available samples of lubricants (RSD <= 12%).
引用
收藏
页码:719 / 722
页数:4
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